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Effects of phosphogypsum whiskers modification with calcium stearate and their impacts on properties of bleached softwood paper sheets, TAPPI Journal September 2021
ABSTRACT: By combining the structural properties and characteristics of phosphogypsum whiskers, a preliminary study on the modification of phosphogypsum whiskers and their application in papermaking was carried out. The effects of reaction temperature, reaction time, and reaction concentration on the solubility and retention of modified phosphogypsum whiskers and the effects of phosphogypsum whiskers on the physical properties of paper under different modified conditions were explored. The research results show that, after the phosphogypsum whiskers are modified with calcium stearate, a coating layer will be formed on the surface of the whiskers, which effectively reduces the solubility of the phosphogypsum whiskers. The best modification conditions are: the amount of calcium stearate relative to the absolute dry mass of the phosphogypsum whisker is 2.00%; the modification time is 30 min, and the modification temperature is 60°C. The use of modified phosphogypsum whiskers for paper filling will slightly reduce the whiteness, folding resistance, burst resistance, and tensile strength of the paper, but the tearing degree and retention of the filler will be increased to some extent.
Journal articles
Magazine articles
Critical parameters for tall oil separation I: The importance of ration of fatty acids to rosin acids, TAPPI Journal September 2019
ABSTRACT: Tall oil is a valuable byproduct in chemical pulping of wood, and its fractions have a large spectrum of applications as chemical precursors, detergents, and fuel. High recovery of tall oil is important for the economic and environmental profile of chemical pulp mills. The purpose of this study was to investigate critical parameters of tall oil separation from black liquor. To investigate this in a controlled way, we developed a model test system using a “synthetic” black liquor (active cooking chemicals OH- and HS- ions), a complete process for soap skimming, and determination of recovered tall oil based on solvent extraction and colorimetric analysis, with good reproducibility. We used the developed system to study the effect of the ratio of fatty acids to rosin acids on tall oil separation. When high amounts of rosin acids were present, tall oil recovery was low, while high content of fatty acids above 60% significantly promoted tall oil separation. Therefore, manipulating the content of fatty acids in black liquor before the soap skimming step can significantly affect the tall oil solubility, and hence its separation. The findings open up chemical ways to improve the tall oil yield.
Journal articles
Magazine articles
A new technique for the measurement of show-through mottle of fine paper, TAPPI Journal September 2019
ABSTRACT: Mottling within print-through and show-through is caused by the variability of the local optical properties of the sheet. This mottling is visually disturbing and a mark of poor paper quality. The ability to predict print-through mottle of printed paper by measuring show-through mottle on the unprinted sheet would be a valuable asset for paper machine control.We examined the relationship between print-through mottle and show-through mottle. We worked with nine samples of 60 lb. uncoated fine paper (90 g/m2), from various North American paper companies, that were printed on an offset press, 400K (400% Black), on both sides. A show-through mottle instrumental determination technique was developed using an existing Fast Fourier Transform-based algorithm. The nine samples examined were ranked similarly by the visual evaluation of print-through mottle and by the instrumental determination of show-through mottle. We thus established that show-through on the unprinted sheet can be used as a reliable predictor of print-through, therefore saving time and money for papermakers. We also found a significant two-sidedness in show-through for some of the samples.
Journal articles
Magazine articles
Dielectric spectroscopic studies of biological material evolution and application to paper, TAPPI JOURNAL September 2018
Dielectric spectroscopic studies of biological material evolution and application to paper, TAPPI JOURNAL September 2018
Journal articles
Magazine articles
Progress in foam forming technology, TAPPI JOURNAL August 2019
ABSTRACT: This paper summarizes recent developments in foam forming that were mainly carried out in pilot scale. In addition to improving the efficiency of existing processes and allowing better uniformity in material, a wide variety of raw materials can be utilized in foam forming. The focus of this paper is thin webs—papers, boards and foam-laid nonwovens, along with the pilot scale results obtained at VTT in Finland. For paper and board grades, the most direct advantage of foam forming is the potential to produce very uniform webs from longer and coarser fibers and obtain material savings through that. Another main point is increased solids content after a wet press, which may lead to significant energy savings in thermal drying. Finally, the potential to introduce “difficult” raw materials like long synthetic or manmade fibers into a papermaking process enables the manufacturing of novel products in an existing production line. This paper also briefly discusses other interesting foam-based applications, including insulation and absorbing materials, foam-laid nonwovens, and materials for replacing plastics.
Journal articles
Permeability simulation for filled paper based on three-dimensional structural model developed by X-ray computed tomography scanning, TAPPI Journal March 2026
ABSTRACT: In this study, an in-depth exploration of filled paper was conducted to understand its structural and permeability characteristics. Cotton linter pulp and precipitated calcium carbonate (PCC) filler were utilized to prepare pure fiber paper, and PCC1 and PCC2 filled papers with different filler particle sizes. Then, the pore structure parameters of paper samples were characterized by mercury intrusion porosimetry, and the X-ray computed tomography (X-CT) scanning was carried out. Subsequently, the 3D microstructures were established based on the X-CT slice images, and the filler characteristic parameters and filler 3D distribution were quantitatively analyzed. Finally, permeation simulations in the thickness and horizontal directions were performed. The findings indicate that filling changes the paper porosity, and the pore tortuosity varies with direction. The estimated pore•throat radius distribution shows specific patterns for different papers. The fillers have different distribution characteristics in the paper samples. Moreover, the paper permeability differs with direction, with smallsized filler having a significant impact on fluid penetration in the thickness direction. Overall, this study provides an effective method for investigating internal paper filler and its distribution, which contributes to the understanding of paper structure•performance relationships.
Journal articles
Effects of in-plane straining on the out-of-plane delamination properties of paperboard, TAPPI Journal March 2026
ABSTRACT: Delamination strength is an essential property for the creasing and folding operations of paperboard into boxes. Due to fixation during creasing, the paperboard suffers in-plane straining. In the present study, we aim to increase our understanding of how in-plane straining affects the delamination properties of paperboard. Samples of paperboard were first strained in in-plane tensile loading, both in the machine-direction and in the cross-direction. Afterward, the paperboard is loaded in the out-of-plane (ZD) direction. Three different grades of commercial paperboard from two major manufacturers were tested in a climate-controlled lab. The results showed similar results for all grades of paperboard, with the delamination strength and the out-of-plane stiffness decreasing virtually linearly with pre-straining. With about 5% plastic in-plane straining, the strength was reduced by about 20% and the stiffness decreased by more than 50% for all grades of paperboard. Normalizing the strength and the stiffness with their values without pre-straining reveals virtually the same relation for all grades of paperboard. If proven to be a general result, this will prove valuable in reducing the demand for experiments.
Journal articles
Influence of base sheet properties on barrier coating performance, TAPPI Journal November 2025
ABSTRACT: Paper packaging offers a sustainable alternative to standard plastic-based materials, particularly for food and beverage applications. With reduced fiber treatment options like fluorochemicals, uncoated base stock often provides little-to-no effective barrier against liquid water, oil/grease, or moisture transmission. Despite the lack of natural barrier performance, base sheet properties can significantly influence the efficiency of applied waterbased barrier coatings. In this study, various base stock properties, such as caliper, porosity, roughness, and ash content, are reported to influence the barrier performance of styrene-acrylic and a copolymer of styrene-butadiene/styrene-acrylate based barrier coatings. These findings will help paper and board producers design better, more cost-effective, purposebuilt substrates for barrier applications in the packaging industry.
Journal articles
A laboratory-scale automated vacuum-assisted device for coating of cellulose nanofibrils onto paper, TAPPI Journal November 2025
ABSTRACT: An automated vacuum-assisted coating system was developed to deposit cellulose nanofibril (CNF) layers onto paper substrates, simulating potential industrial geometries while allowing precise control of web speed (10•20 m/min), vacuum time (up to 30 s), and applicator gap (0.5•0.9 mm). Vacuum assistance makes it possible to obtain coat weights over 5 g/m2 in a single pass and increases solids after coating from less than 10% to over 28%• 30%, reducing drying demand by more than 60%. Coat weights were tuned from 6 to over 11 g/m² by varying suspension solids (0.4•0.6 wt%), line speed, and filtration length (20•40 mm), with strong agreement between experimental data and model predictions. Barrier testing showed Kit test values for double folded samples of 9•12 and Gurley air resistances above 4 × 104 s once coat weights exceeded 7 g/m². Comparable performance was achieved with lower fines content CNF (60%) by increasing coat weight, providing technical flexibility and cost advantages for industrial scale-up.
Journal articles
Magazine articles
On increasing wet-web strength with adhesive polymers, TAPPI JOURNAL February 2020
ABSTRACT: Fiber-fiber adhesion, called “bonding” in the old paper physics literature, is a critical component of the overall strength of dry paper. With freshly formed very wet pulp fiber webs, all evidence suggests there are no fiber-fiber crossings with significant adhesive joint strength. With water removal, a point will be reached where fiber-fiber adhesion starts to contribute to the overall wet-web strength.The literature reveals very few examples of polymers that increase fiber-fiber joint strength in freshly formed webs. Here, we summarize the literature and explain why it is so difficult to promote fiber-fiber wet adhesion with polymers. Nevertheless, ongoing research in areas as diverse as tissue engineering scaffolds and biomimetic adhesives gives clues to future developments. Advances in paper machine engineering have lessened the importance of wet-web strength. By contrast, a critical issue in many of the evolving nanocellulose technologies is the strength of objects first formed by aqueous processing, the green strength—the strength of wet bodies before drying. For exam-ple, 3-D printed nanocellulose objects and ultralow density cellulosic aerogels can be destroyed by capillary forces during drying. There is a need for adhesives that strengthen freshly formed, wet lignocellulosic joints.