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Journal articles
Pre-damping effects on water absorption and drying dynamics in flexographic printing, TAPPI Journal November 2025
ABSTRACT: Optimizing flexographic printability can involve the ink and the substrate, as well as the printing process. It has been widely reported in the literature that controlling topography of the substrate and its porosity are vital for good flexographic printability, especially when using water-based inks. This study focuses on how pre-damping a surface impacts liquid absorption and improves wet trapping (ink on ink with no intermediate drying) in flexographic printing. A Prüfbau universal print tester was adapted to analyze flexographic wet-on-wet ink printing and trapping using yellow and magenta inks for contrast. Slow drying of the first ink layer (yellow) leads to mottle when the second layer (magenta) is applied. The study explores the “wet sponge” hypothesis: a pre-damped surface should absorb liquid faster. The Lucas- Washburn equation describes long-term absorption, but it does not capture short-term uptake, which instead follows a linear dependence on time.
The effect of pulp screening on oxygen delignification of high lignin content pulps, TAPPI Journal October 2025
Application: Yield can be improved and energy demand reduced in the kraft pulping process by terminating cooking at a high kappa number and applying oxygen delignification directly to unscreened pulp. This study demonstrates that oxygen delignification is effective on high-lignin-content pulps without prior screening and without compromising the pulp properties.
Journal articles
Effects of biopolymer coatings on paper permeability and capillarity for paper-based rapid diagnostic test devices, TAPPI Journal September 2025
ABSTRACT: Rapid diagnostic test (RDT) devices are widely used for diagnostics due to their affordability, portability, and user-friendliness. However, conventional assays typically rely on nitrocellulose membranes and plastic casings. These materials raise environmental concerns due to their non-renewable nature, energy-intensive production methods, and poor biodegradability. This study explores the development of fully bio-based RDT substrates using a sustainable alternative: softwoodderived microfibrillated cellulose (MFC), cellulose nanocrystals (CNC), and chitosan as surface modifiers to improve paper properties and enhance RDT sustainability. Cotton filter paper substrates were coated with different biopolymer formulations using a manual blade coater: bleached MFC (BMFC), lignin-containing MFC (LMFC), BMFC combined with CNC, LMFC combined with CNC, and chitosan. Evaluation of the most relevant physical properties concerning RDT performance was conducted, including wetting, water retention value, air permeability, capillary flow rate, and surface morphology. Results showed that biopolymer- based coatings can effectively modify surface properties by reducing pore size and tuning hydrophilicity, while maintaining the renewable and bio-based characteristics of the substrate. The LMFC-coated paper exhibited the best overall performance among all formulations, reducing flow time by 50% (3.00 mm/s vs. 1.5 mm/s) compared to the uncoated paper, yet preserving high water retention. The BMFC+CNC coating also significantly improved flow rate, showing a 36.7% reduction (2.37 mm/s vs. 1.5 mm/s), and enhanced porosity uniformity. In contrast, the flow rate of chitosan-coated paper decreased by over 5,000% (0.027 mm/s), reflecting its strong barrier properties and hydrophobic surface (highest contact angle: 91.4°). These findings suggest that MFC-based coatings are promising ecofriendly alternatives to nitrocellulose, offering optimized capillary transport and structural adaptability. This paves the way for the development of sustainable, high-performance, rapid diagnostic tests.
Journal articles
In-situ process monitoring in deep-drawing of paper using partially transparent tools, TAPPI Journal August 2025
ABSTRACT: The production of three-dimensionally formed packaging from paper by deep drawing usually leads to the occurrence of wrinkles, which result from the high tangential compressive stresses in the flange area and the limited flowability of the material. Wrinkles, although mostly tolerated in industry, end in both a reduced visual appearance and a reduction in usability for packaging, as with, for example, when gas-tightness is required. Previous research efforts have been limited to determining the wrinkle distribution after completion of forming and removal of the formed part. Consequently, the possibility of understanding the sequence of formation of individual wrinkles in the inhomogeneous material is lost. To remedy this situation, a method for local in-situ process monitoring is presented. Using a transparent die and an industrial camera, the flange area can be observed during the forming process. An image processing algorithm is applied to analyze the local development of the deep drawing process from the continuously recorded image data. The method described can be used to analyze the draw-in behavior and wrinkle formation locally and continuously over the drawing depth. The blank holder force influences the draw-in and the wrinkle pattern both locally and throughout the drawing process. A more precise understanding of the wrinkle formation will allow for more efficient process control in the future.
Journal articles
Colloidal silica and its effects during formation of paper sheets in the presence of nanofibrillated cellulose, cationic starch, and cationic acrylamide copolymer, TAPPI Journal May 2025
ABSTRACT: This work considered effects of colloidal silica addition during laboratory preparation of paper sheets containing nanofibrillated cellulose (NFC) that had been pretreated with cationic starch. The emphasis was on process performance issues, including dewatering rates, fine particle retention, and the extent of fiber flocculation. In addition, micrographs were obtained to show what was happening to the NFC upon treatments with cationic starch and subsequent application of hydrodynamic shear. Contrasting results were obtained, depending on the charge density of the cationic starch. Pretreatment of the NFC with a high charge density cationic starch (degree of substitution 0.2) resulted in strong interactions with the colloidal silica, enhancing the dewatering rate and contributing to fine-particle retention. The medium charge cationic starch pretreatment led to effects suggesting a bridging mechanism of action, and subsequent colloidal silica had no significant effect on dewatering. Treatment of that system with a high level of colloidal silica (0.2%) resulted in lower retention. In general, the final colloidal silica treatments tended to decrease the level of flocculation in the suspensions, giving more uniform handsheets. Mechanisms, some of them related to the clustering and dispersion of cationic starch-treated NFC, were proposed to account for the observed effects.
Journal articles
Magazine articles
Numerical analysis of the impact of rotor and screen hole plate design on the performance of a vertical pulper, TAPPI Journal April 2025
ABSTRACT: The dissolving of mechanical pulp is one of the most important process steps in stock preparation, since pulping occurs at the very beginning of the papermaking process. Efficient mixing of the pulp in a short amount of time is essential to achieve high furnish volume flow rates. The design of the rotor, as well as the pulper vat and inserts, significantly affects the overall performance of the pulper, such as mixing efficiency and power demand. Using advanced numerical methods such as computational fluid dynamics (CFD) can accelerate the development process. The CFD simulations allow for detailed analysis of flow phenomena, making it possible to study a real-size machine numerically. This approach is particularly advantageous because it can reduce the need for timeconsuming and costly experiments associated with scaling up test rigs. In this study, we compared two different rotor designs utilized in a vertical pulper and evaluated the numerical results with experimental data. Rotor A is designed for low turbulence and low power demand, while rotor B is designed for high turbulence with high power demand. The CFD results showed good agreement with the experimental measurements. We investigated how the rotor design influences the free fluid surface and the mixing efficiency. Our study also highlights the differences in results depending on whether water or furnish is simulated, which exhibit Newtonian or, respectively, non-Newtonian fluid behavior. Additionally, a detailed numerical investigation of various screen hole plate designs revealed that the newly developed hole design significantly reduces pressure loss compared to a standard drilled hole. This outcome was consistent for both types of fluids investigated: water and furnish.
Journal articles
Effect of xylan on the mechanical performance of softwood kraft pulp 2D papers and 3D foams, TAPPI Journal March 2025
ABSTRACT: Pulp fibers are paramount in paper products and have lately seen emerging use in fiber foams. Xylan, an integral component in pulp fibers, is known to contribute to paper strength, but its effect on the strength of pulp fiber foams remains less explored. In this study, we investigate the role of xylan in both 2D handsheets and 3D foams. For a softwood kraft pulp, we enzymatically removed 1% from pulp fibers and added 3% xylan to them by adsorption, corresponding to approximately a decrease of a tenth and an increase of a third of the total xylan content. The mechanical properties of 2D fiber networks, i.e., handsheets, made using the xylan-enriched pulp improved, particularly regarding tensile strength and Young’s modulus; however, the decrease in mechanical properties of handsheets made from enzymatically- treated xylan-depleted pulp was more pronounced. In 3D networks • pulp fiber foams, much less fiber-fiber contacts formed, and thus the mechanical properties were not as much influenced by removal of xylan. Furthermore, the presence of the required surfactant on the fibers, acting as debonding agent, overshadows any positive effect xylan might have on fiber-fiber bonding. We propose that the improved mechanical properties for the sheets result from a combination of an increased number of fiber-fiber bonds and higher sheet density, while the deterioration in mechanical properties of handsheets comprising enzymatically-treated fibers is caused by the opposite effect.
Journal articles
Water-based adhesive penetration into paperboard and coated paperboard, TAPPI Journal January 2025
The setting of water-based adhesives in contact with paperboard is important in the production of boxes and other packaging, but the topic has received little attention in the literature. The penetration of the adhesive into the paper surface is important to get good bond strength through mechanical interlocking. The influence of the process conditions and the paper properties on this penetration is lacking. A water-based adhesive was applied to an uncoated and coated paperboard. The coating layer had two latex levels. Samples were characterized in terms of air permeability, void fraction, average pore size, and coat weight. The adhesive was applied to the samples in a mechanical press, squeezing a drop between two samples. The penetration of the adhesive was characterized with a silicone oil absorption method that measured the decrease in pore volume after the adhesive had been applied to approximate the pore volume taken up by the adhesive. The bond strength was measured with a peeling test. The penetration depth into uncoated paper did not depend on the application method parameters such as pressing time, pressure, or initial solids of the adhesive. The penetration depth ranged from 35•40 mm. The penetration into 10 pph latex content coated paper was similar to the uncoated samples, but reduced penetration was observed into the 40 pph latex content coatings. The results were compared to the limiting amount of adhesive that was obtained from the weight gain of the samples and to a simple model that is based on flow in porous media. Peel tests revealed that good penetration was needed, as well as a strong coating layer to obtain high peel forces.
Journal articles
Magazine articles
Effects of different soda loss measurement techniques on brownstock quality, TAPPI Journal July 2024
ABSTRACT: The efficiency of the kraft recovery plant, bleaching process, and paper machine are affected when black liquor carryover from the brownstock washers is not controlled well. Measuring soda loss within a mill can vary from using conductivity, either in-situ or with a lab sample of black liquor filtrate squeezed from the last stage washer, to measuring absolute sodium content with a lab sodium specific ion probe or spectrophotometer. While measuring conductivity has value in tracking trends in black liquor losses, it is not an acceptable method in reporting losses in absolute units, typically in lb/ton of pulp. This is further complicated when trying to benchmark soda loss performance across a fleet of mills with multiple washer lines. Not only do the testing methods vary, but the amount of bound soda on high kappa pulps can be significant. This variability creates inconsistent results, and studies are needed to understand the effect of different testing methods on the pulp quality. In this study, soda loss is expressed as sodium sulfate (Na2SO4). Four different methods to measure soda content in pulp off commercial brownstock washers were studied: full digestion (FD), washing soaking overnight and washing (WSW), soaking in boiling water and stirring 10-min (SW-10), and squeeze-no wash (Sq). Total, washable, and bound sodium sulfate calculations were determined for each soda content measuring technique using inductively coupled plasma-optical emission spectroscopy (ICP-OES). Results showed bound and washable sodium sulfate amounts significantly depend on which soda measurement technique was used. In addition, the soda results were correlated with the pulp kappa numbers. As the kappa number increases, bound soda increases, regardless of the soda measurement method used. Impacts of high sodium sulfate in brownstock are also discussed.
Editorial: The next phase of research in academia and industry, TAPPI Journal September 2023
ABSTRACT: The pulp, paper, and textile sectors have contrib-uted to lifestyle improvements for people with the development and commercialization of products like toilet tissue, facial wipes, diapers, and feminine hygiene products, to name a few. Research and development (R&D) efforts in these sectors are critical now more than ever due to the need for healthcare and lifesaving products, as became evident with the COVID-19 pandemic. Additionally, the need to meet net-zero carbon goals and the necessity to revive manufacturing in devel-oped economies clearly emphasize the requirement to ex-amine the R&D landscape. Academia, industry, and governments have respective roles to play in this field.