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Pareto-based design of experiments for identifying and comparing optimum sealing parameters of heat sealing applications in packaging machines, TAPPI Journal June 2023
ABSTRACT: Sealing is one of the most important process steps in industrial packaging, because the sealed seam is the most sensitive section of a package in terms of quality. For this reason, a major focus in flexible packaging is the sealing process, and among this, heat sealing is the most frequently used technology. In detail, applications of heat sealing processes are confronted with four conflicting objectives: increasing seam quality, reducing dwell time, reducing sealing temperature, and increasing process robustness towards varying conditions. Typical problems, such as identification of the optimum process parameters or selection of the most appropriate packaging film, are subject to these conflicting objectives.This paper presents a recently published design of experiments for characterizing and comparing heat sealing properties of packaging films based on a multi-objective optimization algorithm. The approach provides easy-to-read charts showing all optimum sealing parameters with regard to the four essential objectives of heat sealing: seam quality, dwell time, sealing temperature, and process robustness. Three case studies show exemplary applications of the new approach: 1) analyzing transport damages of beverage powder packages; 2) identifying and comparing optimum sealing parameter of a standard, mono-material, and fiber based packaging film regarding tightness and visual properties of the produced sachets; and 3) analyzing the effect of additional aluminum layers on sealing characteristics regarding hot-tack.The new design of experiments may provide the basis of a standard test method for the identification of optimal sealing parameters in the heat sealing processes.
Journal articles
Magazine articles
Paper bending stiffness and web tension measurement from a running web using a vacuum and computer imaging, TAPPI Journal May 2023
ABSTRACT: A novel method for measuring the bending stiffness of paper online during manufacturing is introduced. The method uses photometric stereo imaging to detect the shape of the deflection surface caused by a controllable pressure difference over the paper’s surfaces. The hardware for the measurement is based on a combination of two existing sensors, which has accelerated and facilitated the development of the implementation. The deflection and loads are tied together by the governing differential equation for the bending of an orthotropic elastic plate with selected simplifications. An approach to resolve material parameters and in-plane loads without knowledge of traditional boundary conditions is suggested. The presented method was tested in a paper mill during manufacturing. For bending stiffnesses measured online, correlation coefficients 0.88 and 0.92 were obtained compared to state-of-the-art laboratory measurements. However, the results gained from a moving web are noisy and the data requires correction of the slope and an off-set. Although several issues remain to be resolved before the method can be considered as an accurate measurement for industrial use, the theoretical background, the performance of online implementation, and the results are promising. Possible causes for the observed discrepancies and the future development of the method are discussed.
Journal articles
Magazine articles
Kraft pulp viscosity as a predictor of paper strength: Its uses and abuses, TAPPI Journal October 2023
ABSTRACT: For bleached kraft pulps, two factors govern paper strength: the individual fiber strength, and the bond strength that adheres the individual fibers together in the paper matrix. Inherent fiber strength is related to the length of the carbohydrate polymers, also known as the degree of polymerization (DP). Average DP (DP) is inferred by performing pulp viscosity measurements. Under certain circumstances during kraft pulping and bleaching, the average polymer lengths can be shortened, resulting in lower pulp viscosity, and may indicate fiber damage. Fiber damage typically manifests itself as a reduction in tear strength for well-bonded handsheets.This paper will review the literature on how pulp viscosity can predict paper/fiber strength and how it can be used as a diagnostic tool. It can be a means to monitor pulp quality during pulping and bleaching, as well as to alert when such operations approach a critical threshold. However, viscosity losses must be carefully and judiciously analyzed. Like most diagnostic tools, viscosity measurements can be misused and abused, which can lead to incorrect inferences about intrinsic fiber strength. This review will also cover these misuses. The overall goal is to provide the papermaker a better understanding of what pulp viscosity is, how it correlates to potential sheet strength, and what its limitations are. It will be illustrated that when pulp viscosity drops below a critical value, it will indicate an appreciable deterioration in the paper’s tear and tensile strength.
Journal articles
Magazine articles
The role of hornification in the deterioration mechanism of physical properties of unrefined eucalyptus fibers during paper recycling, TAPPI Journal February 2024
ABSTRACT: Physical properties of cellulosic paper deteriorate significantly during paper recycling, which hinders the sustainable development of the paper industry. This work investigates the property deterioration mechanism and the role of hornification in the recycling process of unrefined eucalyptus fibers. The results showed that during the recycling process, the hornification gradually deepened, the fiber width gradually decreased, and the physical properties of the paper also gradually decreased. After five cycles of reuse, the relative bonding area decreased by 17.6%, while the relative bonding force decreased by 1.8%. Further results indicated that the physical property deterioration of the paper was closely related to the decrease of fiber bonding area. The fiber bonding area decreased linearly with the reduction of re-swollen fiber width during paper recycling. Re-swollen fiber width was closely related to the hornification. Hornification mainly reduces the bonding area of unrefined eucalyptus fiber rather than the bonding force. The work elucidates the role of hornification in the recycling process of unrefined eucalyptus fibers and the deterioration mechanism of paper physical properties, which will be helpful to control the property deterioration of paper and achieve a longer life cycle.
Journal articles
Effect of xylan on the mechanical performance of softwood kraft pulp 2D papers and 3D foams, TAPPI Journal March 2025
ABSTRACT: Pulp fibers are paramount in paper products and have lately seen emerging use in fiber foams. Xylan, an integral component in pulp fibers, is known to contribute to paper strength, but its effect on the strength of pulp fiber foams remains less explored. In this study, we investigate the role of xylan in both 2D handsheets and 3D foams. For a softwood kraft pulp, we enzymatically removed 1% from pulp fibers and added 3% xylan to them by adsorption, corresponding to approximately a decrease of a tenth and an increase of a third of the total xylan content. The mechanical properties of 2D fiber networks, i.e., handsheets, made using the xylan-enriched pulp improved, particularly regarding tensile strength and Young’s modulus; however, the decrease in mechanical properties of handsheets made from enzymatically- treated xylan-depleted pulp was more pronounced. In 3D networks • pulp fiber foams, much less fiber-fiber contacts formed, and thus the mechanical properties were not as much influenced by removal of xylan. Furthermore, the presence of the required surfactant on the fibers, acting as debonding agent, overshadows any positive effect xylan might have on fiber-fiber bonding. We propose that the improved mechanical properties for the sheets result from a combination of an increased number of fiber-fiber bonds and higher sheet density, while the deterioration in mechanical properties of handsheets comprising enzymatically-treated fibers is caused by the opposite effect.
Journal articles
Predictive advisory solutions for chemistry management, control, and optimization, TAPPI Journal March 2025
ABSTRACT: Process runnability and end-product quality in paper and board making are often connected to chemistry. Typically, monitoring of the chemistry status is based on a few laboratory measurements and a limited number of online specific chemistry-related measurements. Therefore, mill personnel do not have real-time transparency of the chemistry related phenomena, which can cause production instability, including deposition, higher chemical consumption, quality issues in the end-product and runnability problems. Machine learning techniques have been used to establish soft sensor models and to detect abnormalities. Furthermore, these soft sensors prove to be most useful when combined with expert-driven interpretation. This study is aimed at utilizing a hybrid solution comprising chemistry and physics models and machine learning models for stabilizing chemistry-related processes in paper and board production. The principal idea is to combine chemistry/physics models and machine learning models in a fashion close to white box modeling. A cornerstone in the approach is to formulate explanations of the findings from the models; that is, to explain in plain text what the findings mean and how operational changes can mitigate the identified risks. The approach has been demonstrated for several different applications, including deposit control in the wet end, both raw water treatment and usage, and wastewater treatment. This approach provides mill personnel with knowledge of identified phenomena and recommendations on how to stabilize chemistry-related processes. Instead of using close to black box machine learning models, a hybrid solution including chemistry/physics models can enhance the performance of artificial intelligence (AI) deployed systems. A successful way of gaining the trust from mill personnel is by creating a plain text explanation of the findings from the hybrid models. The correlation between the likelihood of a phenomena and disturbance and the explanations are derived and validated by application and chemistry and physics experts.
Journal articles
Colloidal silica and its effects during formation of paper sheets in the presence of nanofibrillated cellulose, cationic starch, and cationic acrylamide copolymer, TAPPI Journal May 2025
ABSTRACT: This work considered effects of colloidal silica addition during laboratory preparation of paper sheets containing nanofibrillated cellulose (NFC) that had been pretreated with cationic starch. The emphasis was on process performance issues, including dewatering rates, fine particle retention, and the extent of fiber flocculation. In addition, micrographs were obtained to show what was happening to the NFC upon treatments with cationic starch and subsequent application of hydrodynamic shear. Contrasting results were obtained, depending on the charge density of the cationic starch. Pretreatment of the NFC with a high charge density cationic starch (degree of substitution 0.2) resulted in strong interactions with the colloidal silica, enhancing the dewatering rate and contributing to fine-particle retention. The medium charge cationic starch pretreatment led to effects suggesting a bridging mechanism of action, and subsequent colloidal silica had no significant effect on dewatering. Treatment of that system with a high level of colloidal silica (0.2%) resulted in lower retention. In general, the final colloidal silica treatments tended to decrease the level of flocculation in the suspensions, giving more uniform handsheets. Mechanisms, some of them related to the clustering and dispersion of cationic starch-treated NFC, were proposed to account for the observed effects.
Journal articles
A systems approach for process debottlenecking towards a sustainable pulp and paper industry, TAPPI Journal April 2026
ABSTRACT: Increasing the competitiveness of the pulp and paper industry requires an effective optimization of its existing assets in line with a long-term vision for process transformation, production upgrade, and product diversification. Currently, pulp production increase is one of the main sources of additional revenue for the kraft industry. Likewise, energy efficiency is often employed as a cost-effective approach to reduce operating costs, enhancing the possibilities to lower fossil fuel consumption and contributing to a low-carbon economy. On the other hand, reaching higher production targets and facilitating process transformation, such as biorefinery implementation, heavily depend on the status and performance of a mill’s current infrastructure; therefore, a system analysis is needed to assess the new production requirements, the bottlenecks, and the interactions across departments. In order to obtain practical improvement solutions, direct and indirect impacts on process performance and resource utilization should be considered. This work provides an overview of the key challenges that need to be addressed for production increase and energy efficiency improvement. The methodology starts by a scope analysis for debottlenecking and screening capacity limitations vs. mill targets, followed by their ranking (bottleneck ranking diagram). Benchmarking, gap analysis, and root-cause techniques are applied to diagnose system inefficiencies. This mill-wide debottlenecking assessment is then used to guide the selection of a long-term sustainable operation and design a portfolio of improvement projects by avoiding cross effects of the short-term projects on the long term. A case study of a kraft pulp mill is used to illustrate the proposed methodology.
Journal articles
Copper-embedded polyvinyl alcohol (PVOH)-based antimicrobial and biodegradable coating for food packaging applications, TAPPI Journal October 2026
ABSTRACT: The food packaging industry increasingly seeks multifunctional, bio-based materials that ensure product safety while supporting strict municipal environmental sustainability goals. This research addresses functional limitations in compostable packaging by developing a polyvinyl alcohol (PVOH)-based antimicrobial and biodegradable coating through precise incorporation of active copper ions. Copper ions were incorporated into a 20% solids-content PVOH matrix at target concentrations of 100, 500, and 1,000 ppm, then applied to paper and polylactic acid (PLA) bioplastic substrates at a target coating weight of 6 g/m². Antimicrobial testing against Escherichia coli and Salmonella spp. using a bacterial overlay agar method demonstrated robust, localized microbial inhibition zones that increased with copper concentration. Biodegradability and industrial compostability were assessed under controlled conditions over 49 days in accordance with ASTM D5338 and ASTM D6400. Uncoated butcher paper controls exhibited 71.90% biodegradation, whereas copper-embedded PVOH-coated paper achieved 83.59%, conclusively demonstrating that integrated metallic ions did not hinder or delay natural macromolecular decomposition. Scanning electron microscopy and elemental analysis verified uniform coating distribution and stable copper dispersion across all treated surfaces. Differential scanning calorimetry revealed minor, predictable modifications to polymer crystallization kinetics without altering macrostructural film integrity. Barrier evaluations (ASTM F1249 and ASTM D3985) confirmed a substantial, highly significant reduction in oxygen transmission rates, whereas the reduction in water vapor transmission rates was not statistically significant due to PVOH’s inherently hydrophilic nature. These findings demonstrate that copper-embedded PVOH coatings provide a highly effective, active antimicrobial defense system while remaining completely compatible with commercial, sustainable industrial composting loops.
Journal articles
Biomass gasification for green ammonia production in kraft mills, TAPPI Journal September 2026
ABSTRACT: As the global energy sector transitions toward net-zero emissions, kraft pulp mills present a compelling opportunity to produce green fuels and achieve net-negative emissions by capturing biogenic carbon, helping offset hard-to-abate sectors. This study explores the techno-economics of integrating biomass gasification for green ammonia production within kraft mills, using KraftSIM modeling to evaluate ammonia production, steam balance, emissions, and utility impacts. The proposed design enables energy and water system integration with the existing mill and allows for a gradual scale-up without disrupting the chemistry and operation of the recovery cycle. Across five scenarios representing different biomass gasification rates ranging from 100 to 1000 bone-dry metric tons per day (BDMT/d), the process yields ammonia at approximately 0.51 metric tons per bone-dry metric ton (t/ BDMT), while generating significant low- and medium-pressure steam and hot water that offset mill utility demands. The incineration of pressure swing adsorption tail gas and ammonia plant purge gas in the power boiler reduces biomass combustion and enhances power boiler efficiency. Economic analysis suggests a net revenue potential of approximately CA$380/BDMT, which could increase with the implementation of biogenic carbon pricing. Overall profitability is strongly influenced by biomass procurement costs, electricity prices, and prevailing green fuel and chemical market premium. This work outlines a practical, near-term decarbonization pathway for kraft mills by coupling green fuel production with potential opportunities for carbon removal.