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A feasibility study of using the organic Rankine cycle for power generation from the flue gases of recovery boilers, TAPPI Journal August 2022
ABSTRACT: Almost 415 tons/h of flue gases with a temperature of 160°C are released to the atmosphere from the recovery boiler of a pulp mill with capacity of 1000 air dried (a.d.) metric tons of pulp per day. This is a large waste heat stream that can be used to generate power, to decrease the operating costs of a pulp mill, and to save carbon dioxide (CO2) emissions. In this work, the feasibility of using an organic Rankine cycle (ORC) with ammonia as the working fluid to generate power from the flue gases of recovery boilers is studied. CHEMCAD and Taguchi methods are used for simulation of the process and for optimization of operating conditions, respectively. The temperature of the ammonia and flue gases at the exit of evaporator, exit pressure of the pump and turbine, and the degree of subcooling of ammonia at the exit of the condenser are five operating parameters that are manipulated to optimize the process. Three different scenarios are defined: minimizing the net power cost, maximizing the ORC efficiency, and maximizing the net profit. Different aspects of these scenarios, such as net power generation, cost, efficiency, and CO2 emission savings are discussed, and optimum operating conditions are reported.
Journal articles
Magazine articles
Causes of poor dregs settling in a green liquor clarifier, TAPPI Journal August 2022
ABSTRACT: A study was conducted to examine the most likely parameters responsible for poor dregs settling at a kraft mill over a 2.5-year period, using multivariate data analysis (MVDA) and machine learning (ML) techniques. The dregs settling behavior seems to be seasonally influenced, implying that wood quality variation can be a factor. The results from the MVDA/ML analysis show that poor dregs settling is correlated to incomplete combustion and/or low load conditions in the recovery boiler, low sulfidity in the causticizing plant, and high flow in the green liquor•weak wash cycle. Compositions of dregs and black liquor were also examined to identify correlations with impaired dregs settling. The results show that poor dregs settling strongly correlates with high silicon (Si) content in dregs and moderately correlates with high iron (Fe) and high aluminum (Al) contents, and with low bulk density in dregs. For mills that experience dregs settling or green liquor filtering issues, regular compositional analyses of dregs, green liquor, weak wash, and black liquor are recommended in order to monitor the dynamics of silicon and other constituents in the recovery cycle.
Journal articles
Investigating the causes of severe economizer tube thinning in a spent sulfite liquor (SSL) boiler, TAPPI Journal August 2026
ABSTRACT: In this study, the causes of tube thinning in the economizer of an ammonia-based spent sulfite liquor (SSL) boiler in a Canadian pulp mill are investigated. The tube thinning was most severe in the upper tube rows of the lowest economizer sections where the tube surface temperature ranges between about 180°C and 210°C. The location, the temperature range, and the results of a tube failure analysis indicate that some form of corrosion- erosion is the main cause for the tube thinning. The process is likely initiated by the formation of potassium bisulfate in tube deposits. We hypothesize that some areas in the economizer, including gaps in tube shields, have allowed for temporary buildup of deposits that were not fully removed by sootblowing. Potassium bisulfate is highly hygroscopic, so it readily absorbs moisture, forming an acidic solution leading to corrosion. The corrosion products are removed by the erosive effects of high velocity gas movement, causing the tube thinning. The high-speed fluid flow may be a result of sootblower action and/or enhanced flue gas velocity due to channeling. The tube thinning eventually leads to perforation and leakage.
Journal articles
Magazine articles
Critical parameters for tall oil separation I: The importance of ration of fatty acids to rosin acids, TAPPI Journal September 2019
ABSTRACT: Tall oil is a valuable byproduct in chemical pulping of wood, and its fractions have a large spectrum of applications as chemical precursors, detergents, and fuel. High recovery of tall oil is important for the economic and environmental profile of chemical pulp mills. The purpose of this study was to investigate critical parameters of tall oil separation from black liquor. To investigate this in a controlled way, we developed a model test system using a “synthetic” black liquor (active cooking chemicals OH- and HS- ions), a complete process for soap skimming, and determination of recovered tall oil based on solvent extraction and colorimetric analysis, with good reproducibility. We used the developed system to study the effect of the ratio of fatty acids to rosin acids on tall oil separation. When high amounts of rosin acids were present, tall oil recovery was low, while high content of fatty acids above 60% significantly promoted tall oil separation. Therefore, manipulating the content of fatty acids in black liquor before the soap skimming step can significantly affect the tall oil solubility, and hence its separation. The findings open up chemical ways to improve the tall oil yield.
Journal articles
Magazine articles
Evaluation of novel drum chipper technology: pilot-scale production of short wood chips, TAPPI Journal October 2019
ABSTRACT: Impregnation of wood chips with acidic pulping liquors is improved when using short chip lengths. If the average wood chip length is too short, conventional chipping technology will generate excess small material, such as pin chips and fines. The possibility of using newly developed drum chipping technology to produce short-length wood chips was evaluated with a pilot drum chipper operating at different drum velocities and in-feed angles. With a drum velocity of 30 m/s, the average wood chip lengths and the combined fractions of pin chips and fines were 24 mm and 3.3%, 22 mm and 4.2%, and 17 mm and 8.5%. The highest fractions of total accept chips (large and small accepts), 89% to 90% without screening, were observed for drum velocities of 30•34 m/s and average wood chips lengths of 21•22 mm. The results indicate the potential of drum chipping technology for producing short wood chips with relatively high fractions of accept chips and tolerable fractions of pin chips and fines.
Journal articles
Magazine articles
Exergy and sensibility analysis of each individual effect in a kraft multiple effect evaporator, TAPPI Journal October 2019
ABSTRACT: The multiple effect evaporator (MEE) is an energy intensive step in the kraft pulping process. The exergetic analysis can be useful for locating irreversibilities in the process and pointing out which equipment is less efficient, and it could also be the object of optimization studies. In the present work, each evaporator of a real kraft system has been individually described using mass balance and thermodynamics principles (the first and the second laws). Real data from a kraft MEE were collected from a Brazilian plant and were used for the estimation of heat transfer coefficients in a nonlinear optimization problem, as well as for the validation of the model. An exergetic analysis was made for each effect individually, which resulted in effects 1A and 1B being the least efficient, and therefore having the greatest potential for improvement. A sensibility analysis was also performed, showing that steam temperature and liquor input flow rate are sensible parameters.
Journal articles
Examination of scoring parameters of corrugated fiberboard, TAPPI Journal August 2026
ABSTRACT: One of the less interrogated aspects of corrugated packaging are scoring and scoring profiles, the intentional localized crushing of flutes to accommodate package folding and closure. This study explores the effect of scoring parameters on box compression test strength (BCT) of two balanced corrugated boards. Scoring differences produced BCT that varied by 10% for one board and less for the other board. Parameters from 4-point bending of scored specimens showed some correlation with BCT, while eccentricity and torsion parameters had less correlation. Different scores produced BCT differences that were not strongly predicted by most standard tests in the current study, implying other tests may be needed to examine the actual boundary conditions on a box during compression. In a few cases, aggressive scoring produced cracked score lines, and those containers had lower BCT than containers with uncracked score lines.
Journal articles
Editorial: New research sheds light on critical processes in the recovery cycle, TAPPI Journal July
The chemical recovery cycle has been called the backbone of a kraft pulp mill, making modern paper production both economically and environmentally sustainable. It regenerates pulping chemicals (primarily sodium hydroxide and sodium sulfide) used to separate wood fibers, allowing them to be reused rather than continuously replaced, while also recovering energy by burning the organic components of black liquor to produce steam and electricity that supply much of the mill’s power needs. In addition, the recovery cycle minimizes waste, reduces emissions, and recovers valuable by-products, creating a highly efficient closedloop system. Without this process, chemical costs, energy consumption, and environmental impacts would increase, making large-scale kraft pulping significantly less economical and sustainable.
Journal articles
Modern NCG practice, TAPPI Journal July 2026
ABSTRACT: New innovations have been put in operation for collection and handling systems of noncondensable gases (NCGs) in modern kraft pulp mills. This work investigates technologies in new pulp mills that aim to achieve the benefits of odor-free processes while enhancing chemical circulation within the mill. It describes and discusses both past and current systems for collecting and handling NCGs. The mills studied have designed and implemented their NCG systems within the past 10 to 15 years. New innovations have emerged, offering promising methods to further reduce occasional sulfurous odor emissions from the kraft process. These methods explore pretreatment and sulfuric gas stream reuse options in process units where these gases are generated or during the transportation of these side streams to their final destruction site. Using modern practices outlined in this paper, malodorous gases can be collected to the extent that a kraft pulp mill is essentially odor-free pending operator errors or major equipment malfunctions. One of the difficult aspects is that NCG systems in kraft mills are often designed case-by-case, as well as by various equipment vendors and with varying numbers of destruction sites. The actual detailed design depends on the chosen layout, process configuration depending on individual equipment purchased, and even on the design practices of individual suppliers.
Journal articles
Magazine articles
Effects of different ammonium lignosulfonate contents on the crystallization, rheological behaviors, and thermal and mechanical properties of ethylene propylene diene monomer/polypropylene/ammonium lignosulfonate composites, TAPPI Journal January 2020
ABSTRACT: Thermoplastic elastomer (TPE), made from ethylene propylene diene monomer (EPDM) and polypropylene (PP) based on reactive blending, has an excellent processing performance and characteristics and a wide range of applications. However, there are currently no reports in the literature regarding the usage of TPE in making composite boards. In this paper, EPDM, PP, and ammonium lignosulfonate (AL) were used as the raw materials, polyethylene wax was used as the plasticizer, and a dicumyl peroxide vulcanization system with dynamic vulcanization was used to make a new kind of composite material. This research studied the influences of the AL contents on the crystallization behaviors, rheological properties, thermal properties, and mechanical properties of the composites. The results showed that the AL content had a noticeable impact on the performance of the composite board. Accordingly, this kind of composite material can be used as an elastomer material for the core layer of laminated flooring.