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Evaluation of soap recovery efficiency from black liquor — analytical tools, TAPPI Journal April 2023

ABSTRACT: Soap skimmings (“soap”) are typically recovered from black liquor in kraft mills that process a high percentage of softwood. In many mills, the recovery of soap is inefficient, negatively impacting performance of evaporators and recovery boilers and resulting in loss of potential revenue. A thorough evaluation of soap recovery performance in a kraft mill requires measurement of soap content in black liquor at various sampling locations, especially around the soap skimmer.The standard laboratory method for evaluating soap content in black liquor is a complex, multi-step process that relies on solvent extraction and titration; most mills send these samples to an outside laboratory for this analysis. In this study, 100 black liquor samples, with a wide range of soap concentrations, were tested by the standard solvent extraction method. After additional dilution, each sample was also tested for surface tension with a bubble pressure tensiometer. The results were found to correlate very closely with the solvent extraction tests results. This alternate method, using surface tension measurements of diluted black liquor samples, produces rapid results and can be easily implemented in most kraft mills, which would facilitate much more frequent in-house evaluations of soap recovery performance.

Journal articles
Open Access
AOX Content of Paper Manufactured with 'Chlorine Free' Pulps

AOX Content of Paper Manufactured with 'Chlorine Free' Pulps, 1995 Papermakers Conference Proceedings

Journal articles
Open Access
Improving Softwood Mechanical Pulp Properties with Ophiostom

Improving Softwood Mechanical Pulp Properties with Ophiostoma Piliferum, 1995 Pulping Conference Proceedings

Journal articles
Open Access
Pressure drop characteristics of steam condensation flow in triangular channels for multi-channel cylinder dryers, TAPPI Journal September 2026

ABSTRACT: This study investigates the condensation pressure drop characteristics of steam in the channels of multi-channel drying cylinders, which remain insufficiently understood. An experimental system was established using a horizontal mini-channel with a triangular cross-section and a hydraulic diameter of 4.09 mm. Flow visualization combined with a high-precision data acquisition system was employed to systematically examine the effects of steam mass flux (10•60 kg/(m²·s)), inlet temperature (110°C•140°C), and cooling water flow rate (100•500 kg/h) on the frictional pressure drop during condensation. The results indicate that the two-phase frictional pressure drop increases with rising steam mass flux but decreases with increasing saturation temperature, while the effect of cooling water flow rate becomes more pronounced under lower temperature conditions. In addition, several existing two-phase flow pressure drop correlations were evaluated against the experimental data. Based on a comparative assessment of eight existing correlations, a new predictive model was developed through regression analysis, achieving a mean absolute percentage error (MAPE) of 19.56%. These findings elucidate the pressure drop mechanism of steam condensation in triangular channels and establish a high-precision predictive model, providing theoretical guidance and a critical tool for the engineering design and energy consumption optimization of multi-channel drying cylinders.

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