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Using multi-method analysis to identify challenging paper machine deposits and defects, TAPPI Journal March 2025
ABSTRACT: Based on its speed and versatility, Fourier transform infrared (FTIR) spectroscopy is the industry’s common starting point for analysis of a paper machine deposit or defect sample. However, certain contaminants and papermaking process additives cannot be precisely identified solely by infrared spectral interpretation. This lack of specificity could lead to a misinterpretation of the composition of the deposit or defect. A multi-method analysis uses data from two or more analytical techniques, including FTIR spectroscopy, microbiological staining/phase contrast microscopy, pyrolysis-gas chromatography/mass spectrometry (Pyro-GC/MS), and scanning electron microscopy-energy dispersive X-ray spectroscopy (SEM-EDX), to produce a more specific assessment of a sample’s composition. This paper discusses the use of a multi-method analysis in deposit and defect analysis and presents several case studies that demonstrate how this comprehensive approach can often produce an interpretation result of greater conviction and value to the papermaker.
Journal articles
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Considerations in managing wastewater odor at pulp and paper operations, TAPPI Journal March 2022
ABSTRACT: Many pulp and paper mills are, at least periodically, faced with the release of odors that can migrate offsite and be considered a nuisance by nearby residents. At chemical pulp mills, perceptible odors associated with reduced sulfur compounds (RSCs) are common, many of which are highly perceptible owing to their low odor thresholds. As releases of RSCs and other odorous substances from production processes are progressively controlled, the proportional contribution from wastewater treatment systems to areal odors can increase. This review paper summarizes important fundamentals of odor generation, source identification, and control. Common odorous substances are identified, and mechanisms for their generation are summarized. Approaches for measuring odorous substances are detailed to enable more effective management, and various odor control strategies are discussed.
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Evaluation of rice straw for purification of lovastatin, TAPPI Journal November 2021
ABSTRACT: Cholesterol synthesis in the human body can be catalyzed by the coenzyme HMG-CoA reductase, and lovastatin, a key enzyme inhibitor, can reduce hypercholesterolemia. Lovastatin can be obtained as a secondary metabolite of Aspergillus terreus ATCC 20542. In this study, rice straw of lignocellulose was used in aeration and agitation bath fermentation in a 1-L flask, and a maximal crude extraction rate of 473 mg/L lovastatin was obtained. The crude extract was treated with silica gel (230–400 mesh) column chromatography. Ethyl acetate/ethanol (95%) was used as the mobile phase, and isolation was performed through elution with various ethyl acetate/ethanol ratios. The highest production rate of 153 mg/L was achieved with ethyl acetate/ethanol in a ratio of 8:2. The lovastatin gained from the crude extract was added to 12 fractions treated with 0.001 N alkali, and acetone was then added. After 24 h of recrystallization at 4°C, the extract underwent high-performance liquid chromatography. The purity had increased from 25% to 84.6%, and the recovery rate was 65.2%.
Journal articles
Magazine articles
Effects of different ammonium lignosulfonate contents on the crystallization, rheological behaviors, and thermal and mechanical properties of ethylene propylene diene monomer/polypropylene/ammonium lignosulfonate composites, TAPPI Journal January 2020
ABSTRACT: Thermoplastic elastomer (TPE), made from ethylene propylene diene monomer (EPDM) and polypropylene (PP) based on reactive blending, has an excellent processing performance and characteristics and a wide range of applications. However, there are currently no reports in the literature regarding the usage of TPE in making composite boards. In this paper, EPDM, PP, and ammonium lignosulfonate (AL) were used as the raw materials, polyethylene wax was used as the plasticizer, and a dicumyl peroxide vulcanization system with dynamic vulcanization was used to make a new kind of composite material. This research studied the influences of the AL contents on the crystallization behaviors, rheological properties, thermal properties, and mechanical properties of the composites. The results showed that the AL content had a noticeable impact on the performance of the composite board. Accordingly, this kind of composite material can be used as an elastomer material for the core layer of laminated flooring.
Journal articles
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Root cause analysis of cationic polymer additive efficiency decline in virgin and recycle containerboard mills, TAPPI Journal January 2020
ABSTRACT: It is well known that retention, drainage and strength polymers struggle to perform (if at all) in virgin containerboard mills. In-depth studies have been undertaken in this area for more than seven years, investigating the issue from all directions. A key finding of this work is that soluble lignin is detrimental to chemical efficiency. A strong correlation exists between decreased chemical efficiency and high soluble lignin. Both recycled systems and virgin systems have been studied, and this correlation holds true regardless of furnish. The primary area of concern is virgin container-board, because these mills tend to have the highest lignin levels. Some highly closed recycled mills can also build elevated lignin levels that can negatively affect chemical efficiency.
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Multiple recycling of paperboard: Paperboard characteristics and maximum number of recycling cycles— Part I: Multiple recycling of corrugated base paper, TAPPI Journal November 2019
ABSTRACT: Paper for recycling is an important fiber source for the production of corrugated base paper. The change in production capacity toward more and more packaging papers affects the composition of paper for recy-cling and influences the paper quality. This research project investigated the influence of the multiple recycling of five different corrugated base papers (kraftliner, neutral sulfite semichemical [NSSC] fluting, corrugating medium, testliner 2, and testliner 3) on suspen-sion and strength properties under laboratory conditions. The corrugated board base papers were repulped in a low consistency pulper and processed into Rapid-Köthen laboratory sheets. The sheets were then recycled up to 15 times in the same process. In each cycle, the suspension and the paper properties were recorded. In particular, the focus was on corrugated board-specific parameters, such as short-span compression test, ring crush test, corrugat-ing medium test, and burst. The study results indicate how multiple recycling under laboratory conditions affects fiber and paper properties.
Journal articles
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Rewet in wet pressing of paper, TAPPI JOURNAL September 2018
Rewet in wet pressing of paper, TAPPI JOURNAL September 2018
Journal articles
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Citrus-based hydrocolloids: A water retention aid and rheology modifier for paper coatings, TAPPI Journal July 2019
ABSTRACT: The rheological and dewatering behavior of an aqueous pigmented coating system not only affects the machine runnability but also affects the product quality. The current study describes the use of natural hydrocol-loids derived from citrus peel fibers as a rheology modifier in paper coating applications. The results were compared with carboxymethyl cellulose (CMC) in a typical paper coating system. Water retention of the coating formulation was increased by 56% with citrus peel fibers compared to a default coating, and it also was higher than a CMC-containing coating. The Brookfield viscosity of paper coatings was found to increase with citrus peel fibers. Compared to CMC, different citrus peel fibers containing coating recipes were able to achieve similar or higher water retention values, with no change or a slight increase in viscosity. Coatings were applied on linerboard using the Mayer rod-coating method, and all basic properties of paper were measured to assess the impact of citrus peel fiber on the functional value of the coatings. Paper properties were improved with coated paper containing citrus peel fibers, including brightness, porosity, smoothness, surface bonding strength, and ink absorption.
Journal articles
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The evolution of reel statistical methods, TAPPI Journal June 2019
ABSTRACT: Multiple statistical methods for calculating the variance partition analysis (VPA) of reel data have existed for decades. In the paper industry, VPA is also commonly known as reel statistics. VPA commonly consists of total variance (TOT) that is then divided into three components: cross direction (CD), machine direction (MD), and residual (RES). A common mathematical procedure is referred to as ANOVA (analysis of variance). TAPPI Standard Test Method T 545 “Cross-machine grammage profile measurement (gravimetric method)” addresses paper testing and includes the ANOVA equations that have also been used to analyze scanning data.In the 1990s, TAPPI published TIP 1101-01 “Calculation and partitioning of variance using paper machine scanning sensor measurements,” which contained simple formulas that were easy to implement and could be used by a nov-ice to generate statistics on a spreadsheet. All involved quality control system (QCS) suppliers agreed to support this common method in their QCS. TIP 1101 was recently revised, and this paper concerns the analysis of data collected from a scanning sensor in a QCS and the creation of a common method for the calculation of reel statistics by TAPPI’s Process Control Division.
Journal articles
Magazine articles
Contrasting underlying mechanisms of different barrier coating types, TAPPI Journal January 2018
Contrasting underlying mechanisms of different barrier coating types, TAPPI Journal January 2018