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Journal articles
Open Access
Comparative evaluation of conical and double disk refiners: Effects of operating mode, refining intensity, and device geometry on energy consumption and paper properties, TAPPI Journal August 2026

ABSTRACT: This study investigates the effects of refiner operating mode and refining intensity adjusted via pulp flow rate, applied power, and refiner speed on the refining characteristics of high-yield southern softwood. We compared Valmet’s OptiFiner PRO (conical) and DD6700 (double disk) refiners under matched specific edge load (SEL) conditions. Batch and one-pass modes were evaluated for their impact on energy efficiency and physical paper properties. The results showed that while SEL provides a useful baseline, it does not fully account for differences in refiner geometry, particularly angular parameters. With the chosen plate sets, C-factor analysis revealed that the OptiFiner PRO delivers a lower number of fiber impacts at a higher intensity per impact compared to DD6700 at similar SEL, influencing fiber length, short-span compression test (STFI) index, and tear strength development. These findings offer actionable insights for mills seeking to optimize refining efficiency and cost. In summary, conical refiners may provide advantages in compression strength at mid-range energies, while double disk refiners maintain higher tear strength at elevated energies due to better fiber length preservation.

Journal articles
Open Access
Simplified modeling of a complete rotary lime kiln at a pulp mill, TAPPI Journal February 2026

ABSTRACT: Rotary lime kilns are essential and complex components in pulp mills using the kraft process. They are primarily used to produce lime (CaO), which is then employed to make white liquor, the reagent used to separate wood fibers. To understand and improve the performance of the kiln, modeling its behavior is essential. However, the kiln operates through a complex combination of thermal and chemical phenomena. That is why a simplified approach was used to tackle this challenge. A zero/one-dimensional steady-state analysis was performed based on first principles to simplify the modeling process and reduce the need for experimental data. Additional assumptions, such as steady-state operation and the absence of a refractory lining, were introduced to further simplify the model so that it can be used for daily analysis. Moreover, the auxiliary equipment of the plant, such as the intercooler and preheat cyclone, is also modeled. The final model was validated using data from the literature and a two-month analysis of experimental measure-ments from the Burgo Ardennes lime kiln in Virton, Belgium. It shows good agreement with the available data, with a 6% deviation for the adiabatic flame temperature and a 17% average error in predicting the kiln shell outside temperature. For the fuel and lime flow rate predictions, also validated over the same two-month period, the errors were -6.6% and 0.6%, respectively.

Journal articles
Open Access
Development of a packaging test method, TAPPI Journal February 2026

ABSTRACT: Innovation in packaging design will be facilitated by a simple test method to indicate whether a product is compatible with paper recycling. Three laboratories cooperated on the development of a method and used it on linerboard, coated paperboard, wet-strength paperboard, and white copy paper. This test method includes pulping and screening. The data presented here illustrate the factors affecting the results of a bench-scale test. Our observations show that a bench-scale test can give reproducible results for yield, < 5%. We also present an approach to contaminant assessment based on current published test methods. A specification with a lower limit on yield of 70% and a contaminant level of less than 5,000 particles/kg is proposed.

Journal articles
Magazine articles
Open Access
Perfluoroalkyl and polyfluoroalkyl substances (PFAS) — Fibrous substrates, TAPPI Journal September 2023

ABSTRACT: Perfluoroalkyl and polyfluoroalkyl substances (PFAS) have been implemented during the finishing process of textiles such as upholstery, clothing, personal protective equipment, and sports gear to provide water resistance. Currently, PFAS are still present at quantifiable levels in consumer products and food, even though many companies have started to phase out PFAS treatment with non-toxic water repellant replacements given the possible detrimental health effects suggested by current research. This paper is a detailed review that focuses on how PFAS are implemented in textile production and sources of PFAS contamination during chemical treatments. This review also addresses current legislation on PFAS emissions and trade regulations to decrease exposure of consumers due to toxicokinetics and mechanisms of action through-out the body that are still not well understood. This paper includes a literature review on possible PFAS related health conditions shown from past research and contains suggested toxicity levels, exposure routes, duration, and pathways detailed to the best of our ability.

Journal articles
Magazine articles
Open Access
Cross-flow separation characteristics and piloting of graphene oxide nanofiltration membrane sheets and tubes for kraft black liquor concentration, TAPPI Journal September 2023

ABSTRACT: Dewatering of weak black liquor (WBL) in the kraft cycle by evaporation is highly energy intensive. Membranes are an attractive alternative for energy-efficient dewatering, but existing commercial polymeric or ceramic membranes are either degraded in BL or have high capital costs. Our recent works have demonstrated the engineering of graphene oxide (GO) nanofiltration membranes, their stability and promising performance in BL conditions, and preliminary scale-up into sheets and tubes. Here, we describe in detail the separation characteristics of GO membrane sheets and tubes under real BL conditions and crossflow operation. Recycle-mode piloting of a GO tubular membrane showed average “production flux” of 16 L/m2/h (LMH) and high rejections of lignin (98.3%), total solids (66%), and total organic carbon (83%), with no signs of irreversible fouling identified. A corresponding GO sheet membrane produced an average flux of ~25 LMH and maintained high lignin rejection of ~97% during a slipstream pilot at a kraft mill site using WBL with ~16 wt% total solids (TS). Finally, we piloted a Dow/DuPont XUS1808 polyamide composite reverse osmosis (RO) membrane for last-mile processing of the GO nanofiltration membrane permeate. The RO membrane showed a steady state flux of 19 LMH at 65 bar and produced ~0.02 wt% TS water product, which is highly suitable for reuse in pulp washing operations in the kraft process. The results have strong positive implications for the industrial application of GO membranes in BL concentration and other related applications.

Journal articles
Magazine articles
Open Access
Compression refining: the future of refining? Application to Nordic bleached softwood kraft pulp, TAPPI Journal August 2024

ABSTRACT: A new compression refining technology based on the kneading of high consistency pulp has been selected and tested in various conditions with a model Nordic bleached softwood kraft (NBSK) pulp. The method uses a kneader mixer referred to as the ultra continuous mixer (UCM) to condition the pulp. Its performance levels were also compared with those obtained with traditional low consistency (LC) refining of the same pulp.Compression refining of the NBSK pulp with the UCM led to a much better °SR/strength compromise than conventional LC refining. High strength properties can also be achieved by compression refining, in a range similar to/or better than LC refining. The higher the strength required, the greater the advantages of this technology: for a given strength, a difference of up to 10°SR can be obtained as compared to LC refined pulp. Moreover, a higher tear index can be obtained with compression refining, since fiber cutting is greatly reduced.The lower °SR is due to the release of fewer cellulosic fines, which also results in the manufacturing of new papers combining a high strength and a high permeability that cannot be obtained with traditional LC refining. Indeed, with LC refining, a high strength is generally associated with a low permeability. Upscaling this technology seems to be possible since large production devices are already on the market for applications other than paper/pulp. With this new pulp behavior, papermakers will have to learn to think differently, as paper strength and °SR can now be decorrelated.

Journal articles
Magazine articles
Open Access
Dynamic out-of-plane compression of paperboard — Influence of impact velocity on the surface, TAPPI Journal February 2024

ABSTRACT: Processes that convert paperboard into finished products include, for example, printing, where the paperboard is subjected to rapid Z-directional (ZD) compression in the print nip. However, measuring and evaluating the relevant properties in the thickness direction of paperboard are not necessarily straightforward or easy. Measuring at relevant, millisecond deformation rates further complicates the problem. The aim of the present work is to elucidate some of the influences on the compressive stiffness. Both the initial material response and the overall compressibility of the paperboard is studied. In this project, the effect on the material response from the surface structure and the millisecond timescale recovery is explored.The method utilized is a machine called the Rapid ZD-tester. The device drops a probe in freefall on the substrate and records the probe position, thus acquiring the deformation of the substrate. The probe is also allowed to bounce several times on the surface for consecutive impacts before being lifted for the next drop. To investigate the time dependent stiffness behavior, the probe is dropped several times at the same XY position on the paperboard from different heights, thus achieving different impact velocities. The material response from drops and bounces combined allows study of the short-term recovery of the material. The material in the study is commercial paperboard. The paperboard samples are compared to material where the surface has been smoothed by grinding it. Our study shows that there is a non-permanent reduction in thickness and a stiffening per bounce of the probe, indicating a compaction that has not recovered in the millisecond timescale. Additionally, a higher impact velocity has an initial stiffening effect on the paperboard, and this is reduced by smoothing the surface.

Journal articles
Magazine articles
Open Access
Editorial: TAPPI Journal Best Research Paper for 2023 focuses on black liquor concentration using graphene oxide membranes, TAPPI Journal February 2024

ABSTRACT: TAPPI and the TAPPI Journal (TJ) Editorial Board would like congratulate the authors of the 2023 TAPPI Journal Best Research Paper Award and Honghi Tran Prize: Sam Rae, Ella V. Richards, Max Kleiman-Lynch, Brent D. Keller, and Brandon I. Macdonald. Their paper, “Pilot scale black liquor concentration using pressure driven membrane separation,” appeared on p. 223 of the April 2023 issue. This kraft recovery cycle research was recognized by the TAPPI Journal Editorial Board for its innovation, creativity, scientific merit, and clear expression of ideas.

Journal articles
Magazine articles
Open Access
Effects of tissue additives on copy paper forming and properties, TAPPI Journal February 2024

ABSTRACT: Laboratory tests were conducted in an effort to determine the effects on paper machine process attributes and the properties of paper made from recycled copy paper furnish upon the addition of chemical agents that are commonly used in the production of hygiene tissue products. Due to continuing growth in tissue and towel grades of paper, such agents are experiencing greater usage. Charge titration test results revealed that certain dry strength agents associated with tissue manufacturing have the potential to shift the balance of charge in papermaking furnish to less negative or even positive values. Creping adhesive was found to contribute to fine particle retention, especially when present at relatively high levels. Release aid and a polyacrylate dispersant had the opposite effect. Low addition levels of both a creping adhesive and a debonding agent surprisingly increased a wide range of strength attributes of paper handsheets in comparison to sheets prepared from unaltered recycled copy paper furnish. The debonding agent decreased paper strength at higher levels of addition. Such effects appear to depend not only on the expected effects of agents themselves, but also on how they affect the charge balance of the wet-end system.

Journal articles
Magazine articles
Open Access
Effects of carboxymethyl starch as a papermaking additive, TAPPI Journal February 2024

ABSTRACT: Carboxymethyl starch (CMS) is a bio-based, anionic polymer that has potential as part of a dry-strength additive program for papermaking. Due to its negative charge, its effects can be expected to depend on its interactions with various cationic agents. In this work, the effects of CMS were observed following its sequential addition after one of three selected cationic strength agents at different dosage levels. In selected tests, the furnish was pretreated at the 1% level by a dispersant, sodium polyacrylate, which might represent a high level of anionic contaminants in a paper mill system. Laboratory tests were conducted to show the effects on dewatering, fine-particle retention, and flocculation. These tests were supplemented with measurements of charge demand, zeta potential, and handsheet properties. Sequential addition of cationic glyoxylated acrylamide copolymers (gPAM) and CMS were found to strongly promote dewatering. Two gPAM products and a poly(vinylamine) product in sequential addition with CMS were very effective for promoting fine-particle retention. These same sequential treatments of the stock contributed to moderate fiber flocculation, though severe flocculation was caused by further treatment of the furnish with colloidal silica. Handsheet strength results were mixed. In the default recycled copy paper furnish, the average breaking length for the sheets made with cationic additives followed by CMS was not greatly different from the blank condition. Superior strength resulted when the default furnish was treated with a dispersant alone. When the dispersant-contaminated furnish was treated with the same combinations of cationic additives and CMS, the strength returned to the baseline achieved in the absence of the dispersant. The results were discussed in terms of the charged character of the different additives and their interactions not only with the fiber surfaces but also with each other.