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Journal articles
A targeted approach to produce energy-efficient packaging materials from high-yield pulp, TAPPI Journal August 2025
ABSTRACT: Unlike fossil-based plastics, wood-based packaging materials can be produced in an ecofriendly manner using wood chip residuals from sawmills and pulpwood. To produce high-yield pulp like chemithermomechanical pulps (CTMPs) for paperboard and liquid packaging, it is crucial to reduce the electric energy consumption during fiber separation. The ultimate objective is to revolutionize paperboard production by achieving a middle-layer CTMP process that consumes less than 200 kilowatt-hours per metric ton (kWh/t), significantly improving from the current 500•600 kWh/t energy demand. Optimizing the CTMP impregnation process of sodium sulfite (Na2SO3) in wood chips is crucial for achieving uniform softening, ideally at the fiber level. The properties of the fibers are significantly affected by the content of lignin sulfonates within the walls of the fiber and the middle lamellae. In this study, we employed in-house developed X-ray fluorescence (XRF) techniques, validated by beamline measurements, to map the distribution of sulfonated lignin within fibers. It also seemed possible to enhance the surface area of lignin-rich pulp fibers while losing minimal bulk by refining them with well-optimized low consistency (LC) refining. We aimed to achieve a highly efficient separation of coniferous wood fibers by co-optimizing the sulfonation and the temperature in the preheater and chip refiner. Additionally, we explored how lignin’s softening behavior and potential crosslinking influence subsequent unit operations, including pressing, peroxide bleaching, and drying, following the defibration process. In defibration during chip refining, the maximum softening of wood fibers is preferred to maximize fiber preservation and minimize energy consumption. However, optimizing the stiffness of finished pulp fibers is preferable to reduce bulk loss during paperboard production. It can strive to optimize processes to develop stronger, lighter, and more sustainable composite packaging materials. Reducing environmental impact and electric energy can help create a more sustainable future.
Journal articles
Formability and load-bearing capacity of multilayered paperboard in three-dimensional forming, TAPPI Journal August 2025
ABSTRACT: The forming of paper-based products presents significant challenges, including maintaining geometric integrity, managing springback, and overcoming instability limits. These arise from the material properties of paper, with its high anisotropy, inhomogeneity, and limited strain. Multilayered paperboard, formed without adhesives, offers a promising solution. By customizing layer composition and orientation, this approach leverages mutual fiber support to enhance forming properties. Experimental and numerical analyses reveal that adhesive-free bonding during deep drawing enhances the material’s formability and load-bearing capacity and reduces anisotropic springback. These innovations enable superior product protection compared to conventional industrial single-layered paperboard of similar thickness. This study demonstrates the advantages of tailored layer configurations for improved geometric precision and stability, providing a pathway for sustainable, high-performance packaging solutions.
Journal articles
In-situ process monitoring in deep-drawing of paper using partially transparent tools, TAPPI Journal August 2025
ABSTRACT: The production of three-dimensionally formed packaging from paper by deep drawing usually leads to the occurrence of wrinkles, which result from the high tangential compressive stresses in the flange area and the limited flowability of the material. Wrinkles, although mostly tolerated in industry, end in both a reduced visual appearance and a reduction in usability for packaging, as with, for example, when gas-tightness is required. Previous research efforts have been limited to determining the wrinkle distribution after completion of forming and removal of the formed part. Consequently, the possibility of understanding the sequence of formation of individual wrinkles in the inhomogeneous material is lost. To remedy this situation, a method for local in-situ process monitoring is presented. Using a transparent die and an industrial camera, the flange area can be observed during the forming process. An image processing algorithm is applied to analyze the local development of the deep drawing process from the continuously recorded image data. The method described can be used to analyze the draw-in behavior and wrinkle formation locally and continuously over the drawing depth. The blank holder force influences the draw-in and the wrinkle pattern both locally and throughout the drawing process. A more precise understanding of the wrinkle formation will allow for more efficient process control in the future.
Journal articles
On the design of corrugated boards: A new FEM modeling and experimental validation, TAPPI Journal August 2025
ABSTRACT: This study presents a simplified finite element modeling (FEM) approach suitable for large structures made of corrugated boards, such as customized packages, based on a homogenization method, which is combined with correction factors for internal mechanisms. The homogenization process reduces computational time by transforming flute geometries into equivalent elastic models. In large deformations and in the presence of contact for a given geometry, the effective elastic modulus in the thickness direction, as well as the effective thickness of the structure, are corrected by two statistical Weibull distributions representing the contact and buckling mechanisms in a corrugated board. The Weibull parameters are obtained via experimental analysis, and such a process is then validated. The results demonstrate that the statistical parameters (â1 = 0.14, â2 = 1.31) can be used for the simplistic representation of corrugated boards, being computationally efficient. This research contributes to the optimization of corrugated packaging design, specifically by simplifying FEM models for faster, yet equally accurate, simulations.
Journal articles
Editorial: Design considerations for developing high-quality flexible packaging laminates, TAPPI Journal July 2025
ABSTRACT: The global flexible packaging industry has constantly evolved by developing new materials, film design, polymer processing techniques, and machinery to overcome challenges posed by consumer demands, regulation, and societal pressure. While achieving superior quality and improved mechanical film attributes has always been the cornerstone for new technical developments in this industry, the end-of life shortcoming for most plastic films has driven the value chain to strive harder to design and develop sustainable packaging structures.
Journal articles
Adhesion with purpose: The value of primers in sustainable flexible packaging, TAPPI Journal July 2025
ABSTRACT: Primers play a crucial role in flexible packaging by providing adhesion, enhancing performance, and improving the overall quality of packaging structures. As the packaging industry shifts towards more sustainable solutions, it brings new challenges for meeting adhesion requirements. Different types of sustainable materials, with their complicated physical and chemical properties, usually result in poor adhesion in extrusion coating or extrusion lamination, whether this is due to fast crystallization, secondary crystallization, low processing temperature, lack of functional groups, or a combination thereof. Water-based primers ensure that these innovations meet both functional and environmental standards for the packaging of tomorrow. Conventional water-based primers, including polyethyleneimine (PEI) and ethylene acrylic acid (EAA), offer significant advantages in sustainable packaging design by chemically modifying the surface of the substrate to enhance adhesion. In this study, we will discuss adhesion issues in three case studies involving sustainable packaging materials: (1) extrusion coating of polyvinyl alcohol (PVOH) on paper; (2) extrusion lamination of paper and metallized film with starch biopolymer; and (3) extrusion coating of polyhydroxyalkanoates (PHA) on paper. These cases represent three adhesion challenges related to sustainable materials, namely fast crystallization rate, low processing temperature, and secondary crystallization. A three-step adhesion improvement procedure was employed to identify the proper primer in each case study. This procedure included a wetting-out test with primer, an adhesion test, and an extrusion test with priming. In our results, strong fiber tearing or destructive bonds were achieved in each case with the help of water-based primers. These results demonstrate the value of water-based primers in enabling the transition to more sustainable packaging structures without compromising performance.
Journal articles
Editorial: Investing in Amercian advanced manufacturing, TAPPI Journal June 2025
ABSTRACT: American manufacturing is seeing a renewal, which is needed to boost jobs in America, particularly in the middle and manufacturing base of the country. The ongoing tariff situation emphasizes the importance of protecting domestic manufacturing. There is U.S. congressional agreement, in principle, to bring back manufacturing to the United States. However, given how the global trade and manufacturing space has shifted in the last four decades, it may not be a comparative advantage to manufacture low margin and labor-intensive products. Officials in the current U.S. Administration have stated that manufacturing of socks and T-shirts is not necessarily in the interest of the United States, but focusing on value-added products is essential. While silicon chips, solar panels, and batteries are key items of interest, advanced textile materials such as those that find applications in industrial products and composites, products that can save human lives, and products for protecting the environment are highly-valued items that cater to national security.
Journal articles
Conversion of paper-grade pulp from rice straw into dissolving pulp, TAPPI Journal June 2025
ABSTRACT: About 1,165 million metric tons of rice straw is generated every year worldwide, which can be a good source for the circular bioeconomy. In this research paper, the paper-grade pulp from rice straw was converted to dissolving-grade pulp by fractionation in a biorefinery initiative. Rice straw was cooked at an optimum condition of 8% potassium hydroxide (KOH) charge for 120 min at 150°C and produced a pulp yield of 47.2% with a kappa number of 18.5. Subsequently, D0(EP)D1 bleaching was carried out for the produced pulp, and the brightness of the pulp reached to 82.4%. From the black liquor, 16.5% of the lignin and 11.9% of the hemicellulose were isolated for producing biobased products and chemicals, and then the spent liquor was used for soil amendment. The bleached pulp was fractionated in a Bauer McNett fiber classifier. The pulp fibers retained on 16-, 30-, and 50-mesh screens were used as a longer fiber fraction pulp, and pulp fibers retained on 100- and 200-mesh screens were used as a shorter fiber pulp. The longer and shorter fiber fraction pulps were analyzed for cellulose, R10, pentosan, and viscosity. The long fiber fraction pulps were characterized by higher cellulose (88.2% vs. 83.1%) and lower pentosan (11.3% vs. 13.0%) content than the shorter fiber fraction pulps. The longer fiber fraction was further treated with cold KOH to remove residual hemicellulose. The KOH extraction reduced pentosan content in pulp to 6.3% and increased á-cellulose content to 91.3%. The short fiber fraction was converted to monomeric sugars using cellulase enzymes with varying reaction time, temperature, and consistency. The efficiency of cellulase activity was assessed through glucose yield and residual dry weight. A temperature of 45°C, 5.0 pH, 5% consistency, and 6 filter paper units/gram (FPU/g) o.d. pulp resulted in maximum sugar conversion of 85.7%.
Journal articles
The effect of Stachys floridana Shuttlew.ex Benth extract as an additive on the chemical properties of chitosan biodegradable film, TAPPI Journal June 2025
ABSTRACT: The purpose of this study is to explore chitosan with Stachys floridana Shuttlew. ex Benth (SFSB) extract as an additive to prepare an active film. The effects of the SFSB extract on the physical, antioxidant, and bacteriostatic properties of chitosan biodegradable films were studied. The results showed that the addition of SFSB extract significantly improved the antioxidant and antibacterial properties of the film, and its biodegradation rate increased rapidly. Compared to the control film, the water solubility was lower at 19.40%, the expansion degree was higher at 288.90%, the water vapor permeability (WVP) was 0.364 g·mm/(m²·d·kPa), the surface hydrophobicity increased, and the mechanical strength was also improved. The contact angle increased to 89.3°. In addition, as the amount of SFSB increased, the thermal stability of chitosan-Stachys floridana Shuttlew. ex Benth (CS-SFSB) films also increased significantly, and their ultraviolet (UV) blocking ability was gradually enhanced. The results indicate that CS-SFSB has potential as a food packaging material.
Journal articles
Gap mechanics in pulp refiners, TAPPI Journal June 2025
ABSTRACT: Studies of pulp refining have shown that a single bar impact on pulp has only a 1%•5% probability of producing a successful refining effect. This study has explored the reason why. An analysis of refining kinetics suggested that small segments of a fiber length, about a fiber diameter in size, are treated during each impact. Measurements of localized swelling along fiber lengths caused by refining supported this finding. Based on these findings, it was postulated that force transmittal through fiber networks occurred primarily at fiber crossings. The small size of fiber diameters relative to fiber lengths accounts for the low probability of a successful refining event at each impact. This probability, and the probability of fibers being captured and impacted during passage through a refiner, account for the need for multiple bar crossings to refine pulps.