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TAPPI Journal Summaries, Paper360º January/February 2022

TAPPI Journal Summaries, Paper360º January/February 2022

Using bleaching stage models for benchmarking softwood ECF bleach plants, TAPPI Journal July 2022

ABSTRACT: Steady-state bleaching delignification and brightening models were used to gauge how well elemental chlorine-free (ECF) bleach plants were using chlorine dioxide to bleach 25-kappa softwood brownstocks. Case 1 examined the D0(EOP)D1 portion of Mill 1’s five-stage sequence that brightens the pulp to 86% ISO. Case 2 studied the D0(EO)D1 portion of Mill 2’s four-stage sequence, which brightens the pulp to 82% ISO, and Case 3 re-examined the same bleach plant several years after it made improvements around the extraction stage. The models highlighted days in the previously mentioned cases where high bleach usage occurred, presumably because of high brownstock and/or extraction washer carryover, and days where bleach usage was normal. In Case 2, the model esti-mated that 10 kg of the 44 kg chlorine dioxide/metric ton pulp consumed in bleaching was likely reacting with washer carryover sources; approximately two-thirds of this extra consumption was assumed to be reacting with extraction filtrate. Changes that Mill 2 made (Case 3) reduced the unproductive chlorine dioxide usage from 10 to 5 kg/metric ton pulp. When the delignification and brightening models were simultaneously solved, the models predicted somewhat different optimized distributions of chlorine dioxide to D0 and D1 vs. actual values used in bleach plants. However, the forecasted chlorine dioxide totals agreed with the actual values when washer carryover sources were considered. This study showed the bleaching models could be used as hypothetical benchmarks for softwood ECF bleach plants.

On the usage of online fiber measurements for predicting bleached eucalyptus kraft pulp tensile index — an industrial case, TAPPI Journal July 2022

ABSTRACT: Cellulose pulp’s physical-mechanical properties are determined by laboratory tests obtained from prepared handsheets. However, this procedure is time intensive and presents a lead time until the results are available, hindering its utilization for monitoring and decision-making in a pulp mill. In this context, developing real-time solutions for physical-mechanical properties prediction is fundamental. This work applied a mathematical modeling approach to develop a soft sensor for tensile index monitoring. The mathematical model considers online morphology measurements obtained from the last bleaching stage outlet stream and important process variables for tensile index prediction. The results obtained are satisfactory compared to laboratory results, presenting a mean absolute percentual error of 2.5%, which agrees with the laboratory testing method’s reproducibility.

Investigation of the Cellulose-Water Relationship by the Pressure Plate Method, TAPPI Journal July 2022

ABSTRACT: The swelling and water retention properties of pulp fibers are of basic importance in papermaking.

SETPOINT: Let’s Finally Talk About Bruno, Paper360º March/April 2022

SETPOINT: Let’s Finally Talk About Bruno, Paper360º March/April 2022

Efficiency is Key for High Capacities, Paper360º March/April 2022

Efficiency is Key for High Capacities, Paper360º March/April 2022

Improving refining efficiency with deflocculation, TAPPI Journal May 2022

ABSTRACT: The ability to load a refiner requires the formation of a fiber mat between opposing refiner bars. One of the consequences of this is the formation of flocs that persist through the refiner grooves and exit the refiner. These flocs interfere with sheet strength, requiring additional energy to make up the strength deficit. In addition, flocs can initiate string formation, resulting in machine efficiency issues such as cross-machine profile deterioration and the downtime required to correct it. Novel refiner plate modifications have been shown to improve refining efficiency in otherwise identical refiner plates. Energy savings are typically around 15% of gross refining energy on the basis of the treated stock, although much higher reductions have also been seen. Addressing this previously underappreciated flaw in conventional refining enables greenhouse gas reduction and other benefits related to sheet strength and machine efficiency.

TAPPI Journal Summaries, Paper360º November/December 2022

A new method of studying the fundamental mechanisms involved in pigment liberation from recycle papers, TAPPI Journal October 2022

ABSTRACT: Deinking flotation is the most efficient and widely used method of removing ink particles from printed papers to improve the recyclability. A prerequisite for successful deinking flotation is detachment of pigments from paper fibers, a subprocess known as liberation. The degree of liberation is usually determined via hyperwashing tests, which are costly and time consuming. Furthermore, they provide no information on the fundamental mechanisms controlling liberation. In the present work, we developed a new method in which ?-potentials of the particles in a pulp are measured and analyzed. If pigments are not liberated from paper fibers, a frequency distribution plot gives a single peak, while two peaks appear when they are liberated. One can readily determine the degrees of liberation from the peak positions and peak heights. In addition, the ?-potential data can be used to construct disjoining pressure isotherms using the DLVO theory that are useful to better understand the fundamental mechanisms involved and the roles of different reagents used to improve pigment liberation.

Evaluation of soap recovery efficiency from black liquor — analytical tools, TAPPI Journal April 2023

ABSTRACT: Soap skimmings (“soap”) are typically recovered from black liquor in kraft mills that process a high percentage of softwood. In many mills, the recovery of soap is inefficient, negatively impacting performance of evaporators and recovery boilers and resulting in loss of potential revenue. A thorough evaluation of soap recovery performance in a kraft mill requires measurement of soap content in black liquor at various sampling locations, especially around the soap skimmer.The standard laboratory method for evaluating soap content in black liquor is a complex, multi-step process that relies on solvent extraction and titration; most mills send these samples to an outside laboratory for this analysis. In this study, 100 black liquor samples, with a wide range of soap concentrations, were tested by the standard solvent extraction method. After additional dilution, each sample was also tested for surface tension with a bubble pressure tensiometer. The results were found to correlate very closely with the solvent extraction tests results. This alternate method, using surface tension measurements of diluted black liquor samples, produces rapid results and can be easily implemented in most kraft mills, which would facilitate much more frequent in-house evaluations of soap recovery performance.