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Probing the molecular weights of sweetgum and pine kraft lignin fractions, TAPPI Journal June 2021
ABSTRACT: The present investigation undertook a systematic investigation of the molecular weight (MW) of kraft lignins throughout the pulping process to establish a correlation between MW and lignin recovery at different extents of the kraft pulping process. The evaluation of MW is crucial for lignin characterization and utilization, since it is known to influence the kinetics of lignin reactivity and its resultant physico-chemical properties. Sweetgum and pine lignins precipitated from black liquor at different pHs (9.5 and 2.5) and different extents of kraft pulping (30•150 min) were the subject of this effort. Gel permeation chromatography (GPC) was used to determine the number average molecular weight (Mn), mass average molecular weight (Mw), and polydispersity of the lignin samples. It was shown that the MW of lignins from both feedstocks follow gel degradation theory; that is, at the onset of the kraft pulping process low molecular weight-lignins were obtained, and as pulping progressed, the molecular weight peaked and subsequently decreased. An important finding was that acetobromination was shown to be a more effective derivatization technique for carbohydrates containing lignins than acetylation, the technique typically used for derivatization of lignin.
Journal articles
Deinking of inkjet digital nonimpact printing, TAPPI JOURNAL September 2012
Deinking of inkjet digital nonimpact printing, TAPPI JOURNAL September 2012
Journal articles
Magazine articles
Z-direction chemical analysis for new application methods, TAPPI Journal January 2023
ABSTRACT: In conventional wet-end chemical addition during paper production, chemical distribution through the z-direction of the sheet is usually not considered an important characteristic. With a nontraditional chemical dosing approach, such as foam-assisted additive addition, the chemistry can appear at different concentrations throughout the sheet, typically in a z-direction gradient. To fully understand the strength properties of the sheet, it is helpful to view or quantify the chemical distribution through the sheet in the z-direction. One qualitative method uses a dye technique along with confocal laser scanning microscopy to generate an image where the relative chemical concentration can be observed. A quantitative method involves compiling nitrogen analyses of layered subsections of the sheet into a composite graph of relative chemical concentration vs. the z-direction of the sheet. Chemical distribution analysis can be paired with traditional z-direction strength tests, such as Scott bond and z-direction tensile, to help one understand and improve the chemical addition process and its effects.
Journal articles
Magazine articles
Recovery boiler back-end heat recovery, TAPPI Journal March 2023
ABSTRACT: Sustainability and efficient use of resources are becoming increasingly important aspects in the operation of all industries. Recently, some biomass-fired boilers have been equipped with increasingly complex condensing back-end heat recovery solutions, sometimes also using heat pumps to upgrade the low-grade heat. In kraft recovery boilers, however, scrubbers are still mainly for gas cleaning, with only simple heat recovery solutions. In this paper, we use process simulation software to study the potential to improve the power generation and energy efficiency by applying condensing back-end heat recovery on a recovery boiler. Different configurations are considered, including heat pumps. Potential streams to serve as heat sinks are considered and evaluated. Lowering the recovery boiler flue gas temperature to approximately 65°C significantly decreases the flue gas losses. The heat can be recovered as hot water, which is used to partially replace low-pressure (LP) steam, making more steam available for the condensing steam turbine portion for increased power generation. The results indicate that in a simple condensing plant, some 1%•4% additional electricity could be generated. In a Nordic mill that provides district heating, even more additional electricity generation, up to 6%, could be achieved. Provided the availability of sufficient low-temperature heat sinks to use the recovered heat, as well as sufficient condensing turbine swallowing capacity to utilize the LP steam, the use of scrubbing and possibly upgrading the heat using heat pumps appears potentially useful.
Journal articles
Modeling of Bagginess Due to Storage of Paper Reels With Ridges, TAPPI JOURNAL September 2009
Modeling of Bagginess Due to Storage of Paper Reels With Ridges, TAPPI JOURNAL September 2009
Journal articles
Effects of impregnation time on hardwood kraft pulp characteristics and papermaking potential â?¢ a mill study, TAPPI JOURNAL April 2010
Effects of impregnation time on hardwood kraft pulp characteristics and papermaking potential • a mill study, TAPPI JOURNAL April 2010
Journal articles
Superhydrophobic paper coating containing nonconventional clay, TAPPI JOURNAL November 2010
Superhydrophobic paper coating containing nonconventional clay, TAPPI JOURNAL November 2010
Journal articles
Application of AI-based approach to control the papermaking process, TAPPI Journal March 2025
ABSTRACT: This paper explores AI’s role in revolutionizing the pulp and paper industry, and specifically in predicting wet tensile strength (WTS) for specialty-grade papers. Leveraging eLIXA technology, a 90-day study achieved a 15% reduction in chemical dosage and an 80% decrease in wet tensile standard deviation. The real-time dosage prediction led to optimizing the wet strength resin (WSR) consumption and improved process reliability. The self-learning models exhibited adaptability to changing variables, ensuring their robustness. Overall, this study highlights AI’s transformative impact on efficiency, cost savings, and product quality within the dynamic landscape of papermaking. The approach used for wet strength optimization has been used to optimize other aspects of pulp and paper production.
Journal articles
Magazine articles
Editorial: Agility and adaptation in a dynamic business world, TAPPI Journal January 2021
ABSTRACT: As we move into 2020, it's interesting to look back at the research topics that were covered in TAPPI Journal (TJ) the previous year. Members of the TJ editorial board organized diverse special issues on lignin, coating ,forming, and diverse papermaking and biorefinery topics, which are discussed in the following sections.
Journal articles
Adsorption of anionic dissolved and colloidal substances onto calcium carbonate fillers, TAPPI JOURNAL, July 2000, Vol. 83(7)
Adsorption of anionic dissolved and colloidal substances onto calcium carbonate fillers, TAPPI JOURNAL, July 2000, Vol. 83(7)