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Extension of a steady-state chlorine dioxide brightening model for Z-ECF bleaching of softwood kraft pulps, TAPPI Journal March 2021
ABSTRACT: Earlier studies developed a steady-state model to predict the brightness and/or bleach consumption during the chlorine dioxide brightening (D1) of softwood pulps produced by conventional elemental-chlorine-free (ECF) sequences. This model relates the chlorine dioxide consumed to the brightness gains predicated upon an asymptotic D1 brightness limit, an incoming D1 pulp brightness, and an equation parameter (ß11). The current investigation examines the application of this model to ECF sequences that use ozone delignification (Z-ECF). Literature D1 data from various Z-ECF bleaching studies, which investigated OZ, OD0/Z, and OZ/D0 delignification, were fitted to the model. The ß11 parameter was found to be linearly correlated to the entering kappa number. Interestingly, this linear relationship was found to be identical to the relationships observed when modeling the D1 stage for conventional ECF and chlorine-based bleach sequences. Subtle differences in D1 brightening response in the model among the various bleach sequences are reflected by incoming pulp brightness (at the same kappa number). The current model is used to illustrate how alterations to Z-ECF delignification affect D1 brightening and chlorine dioxide consumption.
Journal articles
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Development of converging-diverging multi-jet nozzles for molten smelt shattering in kraft recovery boilers, TAPPI Journal March 2021
ABSTRACT: The effective shattering of molten smelt is highly desired in recovery boiler systems. Ideally, shatter jet nozzle designs should: i) generate high shattering energy; ii) create a wide coverage; and iii) minimize steam consumption. This study proposes a novel converging-diverging multi-jet nozzle design to achieve these goals. A laboratory setup was established, and the nozzle performance was evaluated by generating jet pressure profiles from the measurement of a pitot tube array. The results show that the shatter jet strength is greater with a large throat diameter, high inlet pressure, and a short distance between the nozzle exit and impingement position. Increasing the number of orifices generates a wider jet coverage, and the distance between the orifices should be limited to avoid the formation of a low-pressure region between the orifices. The study also demonstrates that an optimized converging-diverging multi-jet nozzle significantly outperformed a conventional shatter jet nozzle by achieving higher energy and wider coverage while consuming less steam.
Journal articles
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Evaluation of rice straw for purification of lovastatin, TAPPI Journal November 2021
ABSTRACT: Cholesterol synthesis in the human body can be catalyzed by the coenzyme HMG-CoA reductase, and lovastatin, a key enzyme inhibitor, can reduce hypercholesterolemia. Lovastatin can be obtained as a secondary metabolite of Aspergillus terreus ATCC 20542. In this study, rice straw of lignocellulose was used in aeration and agitation bath fermentation in a 1-L flask, and a maximal crude extraction rate of 473 mg/L lovastatin was obtained. The crude extract was treated with silica gel (230•400 mesh) column chromatography. Ethyl acetate/ethanol (95%) was used as the mobile phase, and isolation was performed through elution with various ethyl acetate/ethanol ratios. The highest production rate of 153 mg/L was achieved with ethyl acetate/ethanol in a ratio of 8:2. The lovastatin gained from the crude extract was added to 12 fractions treated with 0.001 N alkali, and acetone was then added. After 24 h of recrystallization at 4°C, the extract underwent high-performance liquid chromatography. The purity had increased from 25% to 84.6%, and the recovery rate was 65.2%.
Journal articles
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Effects of phosphogypsum whiskers modification with calcium stearate and their impacts on properties of bleached softwood paper sheets, TAPPI Journal September 2021
ABSTRACT: By combining the structural properties and characteristics of phosphogypsum whiskers, a preliminary study on the modification of phosphogypsum whiskers and their application in papermaking was carried out. The effects of reaction temperature, reaction time, and reaction concentration on the solubility and retention of modified phosphogypsum whiskers and the effects of phosphogypsum whiskers on the physical properties of paper under different modified conditions were explored. The research results show that, after the phosphogypsum whiskers are modified with calcium stearate, a coating layer will be formed on the surface of the whiskers, which effectively reduces the solubility of the phosphogypsum whiskers. The best modification conditions are: the amount of calcium stearate relative to the absolute dry mass of the phosphogypsum whisker is 2.00%; the modification time is 30 min, and the modification temperature is 60°C. The use of modified phosphogypsum whiskers for paper filling will slightly reduce the whiteness, folding resistance, burst resistance, and tensile strength of the paper, but the tearing degree and retention of the filler will be increased to some extent.
Journal articles
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Recycling performance of softwood and hardwood unbleached kraft pulps for packaging papers, TAPPI Journal February 2023
ABSTRACT: The scope of this work is to evaluate the recyclability potential of hardwood and softwood unbleached kraft pulps, leading to a sound basis for comparison and even to support a decision about fibers accord-ing to the performance achieved. The influence of successive recycling cycles (up to 10 cycles) on the fiber morphol-ogy, pulp suspension drainability, water retention capacity, and handsheet mechanical properties were studied for Eucalyptus globulus and Pinus sylvestris unbleached kraft pulps. The performance of these pulps as linerboard and corrugating medium for packaging was also evaluated. The requirements for brown kraftliner and for high perfor-mance recycled fluting grades is preserved for E. globulus pulp during all 10 recycling cycles, evidenced by the mod-erate decrease of burst index and crush resistance index and by the short-span compression index, whereas the P. sylvestris pulp loses this rating after the second cycle. These results strongly support the higher performance of E. globulus pulp for recycling as compared with softwood kraft pulp from the perspective of packaging papers.
Journal articles
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A fast and non-destructive alternative to the burnout method for paperboard quality inspections using phase-contrast X-ray imaging, TAPPI Journal February 2023
ABSTRACT: An X-ray based quality inspection method for paperboard was implemented and tested as a fast and non-destructive alternative to the burnout method. An argument against X-ray imaging for inspection of paper and paperboard has been that X-ray absorption is low in paper. To overcome this limitation, we used phase-contrast X-ray imaging (PCXI), which gives higher contrast than conventional attenuation-based imaging for low-absorbing materials such as paper. The suggested PCXI method was applied to previously prepared and quality rated samples using the burnout method. A strong similarity between the burnout images and the PCXI images was observed. In conclusion, further development of the phase-contrast X-ray method would provide an interesting option for replacing or complementing the standard burnout method.
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Chemical addition to wet webs using foam application, TAPPI Journal January 2023
ABSTRACT: In papermaking, the conventional way to add chemicals to the web is to dose them into the fiber stock and form the paper afterwards. However, in many cases, adding chemicals directly to the stock is challenging. For example, strength aids tend to increase flocculation in the stock, which limits the addition amounts of those aids. The need for better performance of paper (and paperboard) products has given rise to the need for functionalization of paper. Adding such functional chemicals to the stock is usually rather inefficient. Hence, novel methods are needed to add chemicals to the paper bulk. One such method is dosing chemicals to the wet web via foam application. In this study, we built a laboratory-scale sheetfed dynamic foam application device and utilized it to study addition of starch to wet bleached chemithermomechanical pulp (BCTMP) paper handsheets. The impact of parameters such as vacuum level, the amount of added chemical, and the viscosity of the foaming liquid on the penetration of starch into the wet web was explored. Starch penetration into wet webs was measured via iodine-potassium iodide staining, followed by image analysis. According to our results, controlling the viscosity of the foaming liquid gives the best possibility to control the penetration.
Journal articles
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Z-direction chemical analysis for new application methods, TAPPI Journal January 2023
ABSTRACT: In conventional wet-end chemical addition during paper production, chemical distribution through the z-direction of the sheet is usually not considered an important characteristic. With a nontraditional chemical dosing approach, such as foam-assisted additive addition, the chemistry can appear at different concentrations throughout the sheet, typically in a z-direction gradient. To fully understand the strength properties of the sheet, it is helpful to view or quantify the chemical distribution through the sheet in the z-direction. One qualitative method uses a dye technique along with confocal laser scanning microscopy to generate an image where the relative chemical concentration can be observed. A quantitative method involves compiling nitrogen analyses of layered subsections of the sheet into a composite graph of relative chemical concentration vs. the z-direction of the sheet. Chemical distribution analysis can be paired with traditional z-direction strength tests, such as Scott bond and z-direction tensile, to help one understand and improve the chemical addition process and its effects.
Journal articles
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Editorial: Shaping industry and career success with TAPPI Standards involvement, TAPPI Journal May 2023
ABSTRACT: Within TAPPI, there are many ways to help advance our industry and make sure it thrives for years to come. Writing a research paper for publication or acting as peer reviewer for TAPPI Journal, presenting at a conference or helping to organize one, and becoming involved in the many committees that are part of TAPPI Divisions are just some of the ways. One other very important way to contribute to our industry is through the standards development process.
Journal articles
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Editorial: Critical literature reviews in open source journals, TAPPI Journal June 2023
ABSTRACT: We stand on the shoulders of giants” is a famous metaphor used by Sir Isaac Newton. This testifies to the fact that new information or discoveries are built on understanding and analyzing earlier information. Particularly in science, technology, engineering, and math (STEM) fields, it is important to have thorough analysis of earlier research activities in a particular field to propose a new direction of research, to evolve new ideas, and to develop new test methods and standards. It is a mandatory and required aspect of every original research paper to have a Literature Review section in the introductory part of the paper.