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Dissolution of wood components during hot water extraction of spruce, TAPPI Journal May 2023
ABSTRACT: The purpose of this study was to investigate the autohydrolysis of softwood, which is the main chemical operation in both hot water extraction and steam explosion. Control of the process and monitoring its course were ensured by the careful choice of experimental setup and conditions: a milled spruce material was extracted in a small flow-through reactor to minimize degradation of the dissolved material and to enable analysis of the resulting liquors extracted at selected time points. The obtained liquid and solid fractions were analyzed for sugar composition and acetic acid concentration. The results showed that partially degraded hemicelluloses were extracted; hemicelluloses side chains were cleaved off and detected as monomers, while deacetylation was limited. Chain scissions of cellulose were observed as a result of autohydrolysis.
Journal articles
Black Liquor Recovery by Pressurized, Oxygen-Blown Gasificat
Black Liquor Recovery by Pressurized, Oxygen-Blown Gasification, 1996 Engineering Conference Proceedings
Journal articles
Effects of D0-stage temperature, pH, and kappa factor on chl
Effects of D0-stage temperature, pH, and kappa factor on chlorine dioxide decomposition and D0-(EP)-D1 bleaching performance for eucalypt pulps, TAPPI JOURNAL April 2016
Journal articles
Magazine articles
Use of fines-enriched chemical pulp to increase CTMP strength, TAPPI Journal April 2021
ABSTRACT: In this study, fines-enriched pulp (FE-pulp)—the fine fraction of highly-refined kraft pulp—was benchmarked against highly-refined kraft pulp (HRK-pulp) as a strength agent in eucalyptus chemithermomechanical pulp (CTMP). Both the FE-pulp and the HRK-pulp were produced from unbleached softwood kraft pulp, and equal amounts of those strength agents were added to the original CTMP, as well as to washed CTMP, where most of the fines had been removed. The effects of the added strength agents were evaluated with laboratory handsheets.The FE-pulp proved to be twice as effective as HRK-pulp. Both HRK-pulp and FE-pulp increased the strength of the CTMP handsheets. The bulk of the handsheets decreased, however, as well as the drainability. The addition of 5% FE-pulp resulted in the same strength increase as an addition of 10% HRK-pulp, as well as the same decrease in bulk and CSF. For the handsheets of washed CTMP, the strengths were not measurable; the CTMP lost the sheet strength when the CTMP-fines content was reduced through washing. The reduced strength properties were compensated for by the addition of chemical pulp fines that proved to be an efficient strength agent. The addition of 5% FE-pulp restored the strength values, and at a higher bulk and higher drainability.
Journal articles
Developing a New Paradigm for Linerboard Fillers, TAPPI JOURNAL March 2008
Developing a New Paradigm for Linerboard Fillers, TAPPI JOURNAL March 2008
Journal articles
Biphasic 1-butanol/water delignification of miscanthus for manufacturing papermaking pulp, TAPPI Journal August 2026
ABSTRACT: Miscanthus has emerged as a promising nonwoody fiber source for papermaking and fiber molding as the world has sought alternatives to wood-based products. A diverse range of chemistries have been explored at the laboratory scale to turn nonwoody biomass into fibers; however, few have been successful at pilot or commercial scales. An emerging organosolv delignification chemistry that has demonstrated previous technical success is butanol/water, having been shown to produce papers with similar properties to other, more conventional chemistries, but offering the benefit of a built-in sugar and lignin coproduct separation. While a range of fiber lengths were achieved (0.45•0.95 mm), addition of sodium hydroxide (NaOH) to the butanol/water delignification chemistry resulted in fiber lengths comparable to commercially available hardwood pulps (0.7•1.0 mm). Lignin concentration was reduced from 19.1 wt% in the raw miscanthus to under 3.5 wt% for most trials. The lowest lignin concentration (2.5 wt%) was achieved at 180°C for 180 min with 50:50 butanol:water and 2 wt% acetic acid. Yet, the high severity of this condition (and similar ones) resulted in a significant truncation of fiber length, which is detrimental for papermaking applications. The highest quality pulp for papermaking was generated at 180°C for 180 min with 50:50 butanol:water and 10 wt% NaOH. This pulp had one of the longest fiber lengths, the highest brightness, and the highest hemicellulose concentration. Thus, butanol/water delignification, especially with NaOH addition, resulted in the successful production of cellulose-rich pulps that have potential in commercial papermaking and fiber molding applications.
Journal articles
Optimization of energy efficiency and condensate production in evaporation plants for a modern softwood pulp mill, TAPPI Journal April 2026
ABSTRACT: To meet the need to further improve thermal efficiency and environmental performance of kraft pulp mills, new systems and techniques have been developed within the evaporation plant. This paper describes these novel approaches and how they were implemented in a project completed in 2018 for a new evaporator and condensate treatment system supplied by Valmet at the SCA Östrand market pulp mill in Sweden. This project was part of a stepwise upgrade of the complete mill to increase the production capacity of the mill from 430,000 to 900,000 air-dried metric tons/year (ADt/y). As part of this upgrade, the mill had the objectives to increase the energy efficiency of the pulp mill and to minimize the air emissions as much as possible, the effluent volume, and the water usage in the mill. The mill also wanted to have the disposal of the biosludge in the black liquor, and the production of tall oil from black liquor soap, liquid methanol, and turpentine. This required that the new evaporation and condensate treatment system be very closely integrated into the other process departments of the mill, including integration of the hot weak black liquor flash vapor from the digester directly into the evaporator train and the production of multiple streams of clean evaporation plant condensate at the correct temperature for the bleach plant. Heat and mass balance calculation values, which were found to do very well in predicting the effect on actual mill operation, are also presented in this paper.
Journal articles
Examination of scoring parameters of corrugated fiberboard, TAPPI Journal August 2026
ABSTRACT: One of the less interrogated aspects of corrugated packaging are scoring and scoring profiles, the intentional localized crushing of flutes to accommodate package folding and closure. This study explores the effect of scoring parameters on box compression test strength (BCT) of two balanced corrugated boards. Scoring differences produced BCT that varied by 10% for one board and less for the other board. Parameters from 4-point bending of scored specimens showed some correlation with BCT, while eccentricity and torsion parameters had less correlation. Different scores produced BCT differences that were not strongly predicted by most standard tests in the current study, implying other tests may be needed to examine the actual boundary conditions on a box during compression. In a few cases, aggressive scoring produced cracked score lines, and those containers had lower BCT than containers with uncracked score lines.
Journal articles
Investigating the causes of severe economizer tube thinning in a spent sulfite liquor (SSL) boiler, TAPPI Journal August 2026
ABSTRACT: In this study, the causes of tube thinning in the economizer of an ammonia-based spent sulfite liquor (SSL) boiler in a Canadian pulp mill are investigated. The tube thinning was most severe in the upper tube rows of the lowest economizer sections where the tube surface temperature ranges between about 180°C and 210°C. The location, the temperature range, and the results of a tube failure analysis indicate that some form of corrosion- erosion is the main cause for the tube thinning. The process is likely initiated by the formation of potassium bisulfate in tube deposits. We hypothesize that some areas in the economizer, including gaps in tube shields, have allowed for temporary buildup of deposits that were not fully removed by sootblowing. Potassium bisulfate is highly hygroscopic, so it readily absorbs moisture, forming an acidic solution leading to corrosion. The corrosion products are removed by the erosive effects of high velocity gas movement, causing the tube thinning. The high-speed fluid flow may be a result of sootblower action and/or enhanced flue gas velocity due to channeling. The tube thinning eventually leads to perforation and leakage.
Journal articles
Editorial: New research sheds light on critical processes in the recovery cycle, TAPPI Journal July
The chemical recovery cycle has been called the backbone of a kraft pulp mill, making modern paper production both economically and environmentally sustainable. It regenerates pulping chemicals (primarily sodium hydroxide and sodium sulfide) used to separate wood fibers, allowing them to be reused rather than continuously replaced, while also recovering energy by burning the organic components of black liquor to produce steam and electricity that supply much of the mill’s power needs. In addition, the recovery cycle minimizes waste, reduces emissions, and recovers valuable by-products, creating a highly efficient closedloop system. Without this process, chemical costs, energy consumption, and environmental impacts would increase, making large-scale kraft pulping significantly less economical and sustainable.