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Journal articles
Open Access
Simplified modeling of a complete rotary lime kiln at a pulp mill, TAPPI Journal February 2026

ABSTRACT: Rotary lime kilns are essential and complex components in pulp mills using the kraft process. They are primarily used to produce lime (CaO), which is then employed to make white liquor, the reagent used to separate wood fibers. To understand and improve the performance of the kiln, modeling its behavior is essential. However, the kiln operates through a complex combination of thermal and chemical phenomena. That is why a simplified approach was used to tackle this challenge. A zero/one-dimensional steady-state analysis was performed based on first principles to simplify the modeling process and reduce the need for experimental data. Additional assumptions, such as steady-state operation and the absence of a refractory lining, were introduced to further simplify the model so that it can be used for daily analysis. Moreover, the auxiliary equipment of the plant, such as the intercooler and preheat cyclone, is also modeled. The final model was validated using data from the literature and a two-month analysis of experimental measure-ments from the Burgo Ardennes lime kiln in Virton, Belgium. It shows good agreement with the available data, with a 6% deviation for the adiabatic flame temperature and a 17% average error in predicting the kiln shell outside temperature. For the fuel and lime flow rate predictions, also validated over the same two-month period, the errors were -6.6% and 0.6%, respectively.

Journal articles
Open Access
Physico-mechanical and ethylene scavenging properties of active packaging from Bambusa fibers modified with TiO2 /Cu2O composite, TAPPI Journal February 2026

ABSTRACT: The physico-mechanical and ethylene scavenging properties of active packaging consisting of paper prepared from bamboo (Bambusa vulgaris) fibers loaded with varying concentrations of nano titanium dioxide/cuprous oxide (TiO2/Cu2O) composite was investigated for its ability to delay ripening of Philippine climacteric fruits. Tests of paper containing 1% to 5% TiO2/Cu2O showed no or limited negative impact on its physical, optical, and mechanical properties. Images from a field emission scanning electron microscope equipped with energy-dispersive X-ray spectroscopy (FESEM-EDS) showed dispersion and agglomeration of TiO2/Cu2O nanoparticles on the paper surface. The percent weight of titanium and copper increased with increasing metal oxide composite concentration used in this study. Attenuated total reflection Fourier transform infrared (ATR-FTIR) spectroscopy indicated small shifts in band intensity at 3330 cm-1 and 1100 cm-1 in the hydroxyl (O-H) and C-O regions, respectively, suggesting possible chemical or physical interactions between the metal oxide and paper. Contact angle measurement suggest- ed that TiO2/Cu2O nanoparticles may have imparted paper hydrophobicity at 3% & 5% concentration, possibly through increased microscale roughness. The ethylene scavenging experiment indicated that there was a significant delay in the ripening process of mango and tomato when packed in paper doped with 3% and 5% TiO2/Cu2O. The fruits were greener with a firmer texture compared with untreated control after three days of storage under natural light and ambient condition. The preliminary results suggested that 3% &5% TiO2/Cu2O active packaging modification can remove ethylene from the fruit's storage environment, extending shelf life and maintain quality for three days. This simple technique could have potential economic benefits for the fruit industry by directly reducing post-harvest waste, and the delayed ripening could provide flexibility in supply chain management.

Journal articles
Open Access
Development of a packaging test method, TAPPI Journal February 2026

ABSTRACT: Innovation in packaging design will be facilitated by a simple test method to indicate whether a product is compatible with paper recycling. Three laboratories cooperated on the development of a method and used it on linerboard, coated paperboard, wet-strength paperboard, and white copy paper. This test method includes pulping and screening. The data presented here illustrate the factors affecting the results of a bench-scale test. Our observations show that a bench-scale test can give reproducible results for yield, < 5%. We also present an approach to contaminant assessment based on current published test methods. A specification with a lower limit on yield of 70% and a contaminant level of less than 5,000 particles/kg is proposed.

Journal articles
Editorial: Changing of the guard: Dr. Arthur Ragauskas assumes TAPPI Journal editor-in-chief role, TAPPI Journal January 2026

TAPPI is pleased to announce that Dr. Arthur J. Ragauskas has assumed the editor-in-chief role for TAPPI Journal. Ragauskas, who is a professor at University of Tennessee (UT) in Knoxville, TN, has been a member of the TAPPI Journal Editorial Board since 2011 and is a TAPPI Fellow, as well as recipient of the TAPPI Gunnar Nicholson Gold Medal Award, among his many accomplishments. As a member of the Editorial Board, Ragauskas has curated eight special issues on a range of topics, including nanocellulose, lignocellulose, lignin valorization, and the forest biorefinery.

Journal articles
Full-scale operation of a membrane-based black liquor concentrator, TAPPI Journal January 2026

ABSTRACT: For years, black liquor concentration by reverse osmosis has been an aspiration for reducing mill energy consumption and costs. Building on a 2023 report of an 81% reduction in the energy intensity for concentrating black liquor using its membrane platform at the pilot scale, this paper reports on the fabrication, installation, startup, and operation of the world’s first full-scale membrane-based black liquor concentration system at the International Paper Grande Prairie mill in Canada. The majority of the membrane modules in this system have reliably exceeded permeability expectations by more than 50%. In addition to strong membrane performance, the system has been a significant source of learnings for material specifications and system design. Incorporating these learnings and comparing to typical multiple effect evaporators, the system demonstrates a 43% reduction in capital cost for the same capacity, a 30% reduction in the lifetime cost of removing water from black liquor, and an 86% reduction in energy use. The impact on washer optimization was also considered, and net energy and chemical costs were reduced by US$3.8 and US$6.8/a.d. metric ton for a typical brown and bleach mill, respectively, when incorporating this technology. Completed in less than 12 months, the facility has demonstrated successful black liquor concentration at the 500 gpm scale with monthly uptime as high as 96%.

Journal articles
Energy and emission implications of optimized white liquor causticity, TAPPI Journal January 2026

ABSTRACT: Optimizing the causticizing plant offers significant opportunities for energy and emissions savings in kraft mills by minimizing the chemical and water deadload introduced into the recovery cycle via white liquor. Modern control strategies utilize both feedforward and feedback loops to manage causticity, enabling more aggressive targets closer to equilibrium levels. This paper evaluates the benefits of optimizing white liquor chemistry through a detailed CADSIM Plus simulation model, replicating the chemistry of a Canadian bleached kraft mill that adopted an automated causticizing control system. The control system increased causticity from 77.0% to 82.3% at a fixed total titratable alkali (TTA) of 126.5 grams of sodium dioxide per liter (gNa2O/L). Modeling this chemistry change indicated a 1.5 metric tons per hour (t/hr) reduction in evaporator steam demand and a 2.8% increase in black liquor higher heating value. Consequently, the improved heating value resulted in a 1.5% rise in recovery boiler steam production and a 5.3% reduction in biomass energy consumption in power boilers, leading to a 4.8% decrease in biogenic carbon dioxide (CO2) emissions. Additionally, reducing the inorganic and water deadload throughout the recovery cycle may support higher as-fired dry solids targets, enhancing recovery boiler energy efficiency by lowering the water evaporation requirement during black liquor combustion. However, implementing a causticizing control system requires careful assessment of potential lime kiln bottlenecks, as increased causticity demands may affect kiln operations depending on broader mill conditions. Overall, an automated causticizing control system enhances process efficiency, reduces energy consumption and emissions, and positions kraft mills for improved productivity and longterm sustainability.

Journal articles
Effects of variability of wood chip composition on recovery cycle operation, TAPPI Journal January 2026

ABSTRACT: Fluctuations in wood chip properties in kraft pulp mills, which often follow seasonal patterns, can lead to changes or disruptions in the operation of the recovery cycle whereby the root causes are not immediately obvious. In some cases, these changes are attributed to operational adjustments in the digester or brownstock washing areas resulting from the variability in wood characteristics. Varying wood chip characteristics that have the most significant impact on the recovery cycle operation include the content of non-process elements (NPEs), extractives, and properties influenced by chip storage conditions. Elevated levels of NPEs, often associated with a higher influx of wood bark into the digester, can negatively affect the entire recovery cycle. Increased levels of chlorine and potassium can lead to severe fouling and corrosion in the recovery boiler. Higher concentrations of silicon, aluminum, phosphorus, magnesium and calcium in the chips may accelerate scaling in the evaporation plant, impair dregs and lime mud settling and filtering, reduce lime mud solids content and lime availability, and increase the amounts of dregs, grits, and purged lime mud. This technical review provides an overview of the most significant effects that changes in wood chip quality can potentially exert on various processes within the kraft recovery cycle.

Journal articles
Open Access
Editorial: Advancing the Digital Twin paradigm — From network mechanics to functional paper physics, TAPPI Journal March 2026

This Special Paper Physics Issue of TAPPI Journal serves as a critical bridge between the phenomenological observations shared at the last International Paper Physics Conference in Wuppertal, Germany, and the rigorous quantification required to realize the “Digital Twin” paradigm. This paradigm involves the creation of a virtual dynamic representation of a process that acts as a real-time counterpart of the actual one. We are particularly indebted to Jaan-Willem Simon of the University of Wuppertal, whose leadership was pivotal in translating the conference’s academic rigor into this scholarly collection.

Journal articles
Open Access
Estimating dose and interaction of X-rays with cellulose-based fibrous materials using micro-computed tomography, TAPPI Journal March 2026

ABSTRACT: Micro-computed tomography (ìCT) has a reputation as a nondestructive analysis method. Unfortunately, this leads to the common misconception that radiation damage of the sample does not play a role. With the increased use of ìCT in laboratory-based machines, more and more cellulose-based materials are studied. In this paper, we show with three examples that radiation damage is important in dry and wet paper and in viscose fibers. In an attempt to quantify radiation damage, we came up with a workflow that enables researchers to predict the X-ray dose within a laboratory-based ìCT machine. This gives researchers the possibility to quantitatively judge the influence of radiation damage on each measured sample. While one cannot extend the measured doses from one machine to another, one can still apply the work flow presented in this study to any ìCT setup. In this way, it is possible to minimize radiation damage by choosing the best parameters in a ìCT for obtaining perfect data with no or little radiation damage.

Journal articles
Open Access
Point load measurements on paperboard packages and bulging, TAPPI Journal March 2026

ABSTRACT: Paperboard packaging is made by processing board materials into sheets or rolls and shaping them through creasing, cutting, folding, and erecting. The conversion process generates residual moments at the folds that cause panel bulging. This study experimentally investigates how the bulging introduced during the converting processes influence the mechanical response of paperboard packages during point load testing within the elastic deformation range. The study shows that panel bulging may significantly affect packaging performance as-perceived strength and stiffness. Bulging, influenced by the board’s basis weight, can affect the package performance even more than packaging stiffness. Point load tests in the elastic region were performed on empty packages (78 mm × 50 mm × 110 mm) with force applied at specific points along their long sides. The packages evaluated in this study were made of two identically processed materials of different grammages. The heavier material showed more pronounced bulging than the lighter one, leading to overlapping force-displacement curves for the packages, and to that, a lower force and stiffness may be measured at a certain indentation depth for the package of heavier material. This complicates material choice according to functional requirements. The results show that a highly bulged package might resemble one with less bulging of another material. According to the results, it is not certain that a higher grammage package shows a higher indentation force and stiffness than a lower grammage package when measured at a certain indentation. This indicates that optimizing the creasing and folding processes can be a way to enhance performance rather than simply increasing board weight. The study underscores the importance of controlling converting parameters, especially creasing and folding behavior. Well-performed creasing and folding gives a low residual momentum, little bulging, and a high stiffness and compression strength at point loading in the elastic region. Proper optimization can improve packaging performance and manual handling user-friendliness.