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A Feasibility Study of Using the Organic Rankine Cycle for Power Generation from the Flue Gases of Revcovery Boilers, 2022PEERS/IBBC Conference (22PEE/22IBB)

Green Liquor Clarification Improvements by Utilizing Existing Tanks and Vessels in Mills, 2022PEERS/IBBC Conference (22PEE/22IBB)

INVESTIGATING THE CAUSES OF SEVERE ECONOMIZER TUBE THINNING IN AN SSL BOILER, 2022PEERS/IBBC Conference (22PEE/22IBB)

Cracking of straight co-extruded composite wall tubes in black liquor recovery boilers, 2022PEERS/IBBC Conference (22PEE/22IBB)

Recycled Fiber Paper Mill Water Reduction and Reuse: Reviewing Fresh Water Reduction and Process Water Recycling Initiatives, 2022PEERS/IBBC Conference (22PEE/22IBB)

A feasibility study of using the organic Rankine cycle for power generation from the flue gases of recovery boilers, TAPPI Journal August 2022

ABSTRACT: Almost 415 tons/h of flue gases with a temperature of 160°C are released to the atmosphere from the recovery boiler of a pulp mill with capacity of 1000 air dried (a.d.) metric tons of pulp per day. This is a large waste heat stream that can be used to generate power, to decrease the operating costs of a pulp mill, and to save carbon dioxide (CO2) emissions. In this work, the feasibility of using an organic Rankine cycle (ORC) with ammonia as the working fluid to generate power from the flue gases of recovery boilers is studied. CHEMCAD and Taguchi methods are used for simulation of the process and for optimization of operating conditions, respectively. The temperature of the ammonia and flue gases at the exit of evaporator, exit pressure of the pump and turbine, and the degree of subcooling of ammonia at the exit of the condenser are five operating parameters that are manipulated to optimize the process. Three different scenarios are defined: minimizing the net power cost, maximizing the ORC efficiency, and maximizing the net profit. Different aspects of these scenarios, such as net power generation, cost, efficiency, and CO2 emission savings are discussed, and optimum operating conditions are reported.

Causes of poor dregs settling in a green liquor clarifier, TAPPI Journal August 2022

ABSTRACT: A study was conducted to examine the most likely parameters responsible for poor dregs settling at a kraft mill over a 2.5-year period, using multivariate data analysis (MVDA) and machine learning (ML) techniques. The dregs settling behavior seems to be seasonally influenced, implying that wood quality variation can be a factor. The results from the MVDA/ML analysis show that poor dregs settling is correlated to incomplete combustion and/or low load conditions in the recovery boiler, low sulfidity in the causticizing plant, and high flow in the green liquor•weak wash cycle. Compositions of dregs and black liquor were also examined to identify correlations with impaired dregs settling. The results show that poor dregs settling strongly correlates with high silicon (Si) content in dregs and moderately correlates with high iron (Fe) and high aluminum (Al) contents, and with low bulk density in dregs. For mills that experience dregs settling or green liquor filtering issues, regular compositional analyses of dregs, green liquor, weak wash, and black liquor are recommended in order to monitor the dynamics of silicon and other constituents in the recovery cycle.

Factors affecting deposit formation in foul condensate stripping systems, TAPPI Journal June 2024

ABSTRACT: In kraft pulp mills, foul condensates are often steam-stripped to produce clean condensate for use as process water. The formation of organic deposits in the stripped condensate is a common problem. A systematic study was conducted to examine the deposit composition and the most likely operating parameters responsible for stripped condensate contamination experienced at a kraft mill in Brazil. Daily averaged data of 170 operating parameters over a 15-month period were analyzed by means of multivariate discriminant analysis and random forest classification analysis. The results showed that the deposit formation is related to high temperature, pressure, and dry solids operations in various evaporator effects. These conditions, combined with the poor demisting efficiency in these effects, may have increased black liquor carryover mist in the vapor. Deposit formation also appeared to be related to increased throughput of the foul condensate stripping system and increased pressure in the stripper. Results of Fourier transform infrared spectroscopy (FTIR) and pyrolysis-gas chromatography mass spectrometry (Py-GCMS) analyses show that the deposit consists of mostly organic matter that likely originated from wood extractives and lignin.

Effect of high sulfate content on viscosity of recovery boiler molten smelt, TAPPI Journal March 2024

ABSTRACT: A systematic study was conducted to examine the effect of high sulfate content on the freezing temperature of molten smelt and how this may contribute to the formation of viscous jellyroll smelt in recovery boilers. The results show that even for recovery boilers with a smelt reduction as low as 70%, the sulfate content in smelt has no or little effect on smelt freezing temperature, and hence, on molten smelt fluidity. The perceived adverse effect of high sulfate content on smelt fluidity and on jellyroll smelt formation comes from the high sulfate content in deposits that have fallen from the upper furnace. Fallen deposits may or may not form jellyroll smelt, depending on whether or not they can melt and be well-mixed with molten smelt by the time they reach the smelt spouts. It is not the high sulfate content in smelt resulting from the low smelt reduction efficiency that makes molten smelt viscous and forms jellyroll smelt, but rather, it is the incomplete melting of fallen deposits that results in one of the proposed mechanisms for jellyroll smelt formation.

Editorial: New research sheds light on critical processes in the recovery cycle, TAPPI Journal July

The chemical recovery cycle has been called the backbone of a kraft pulp mill, making modern paper production both economically and environmentally sustainable. It regenerates pulping chemicals (primarily sodium hydroxide and sodium sulfide) used to separate wood fibers, allowing them to be reused rather than continuously replaced, while also recovering energy by burning the organic components of black liquor to produce steam and electricity that supply much of the mill’s power needs. In addition, the recovery cycle minimizes waste, reduces emissions, and recovers valuable by-products, creating a highly efficient closedloop system. Without this process, chemical costs, energy consumption, and environmental impacts would increase, making large-scale kraft pulping significantly less economical and sustainable.