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Pareto-based design of experiments for identifying and comparing optimum sealing parameters of heat sealing applications in packaging machines, TAPPI Journal June 2023

ABSTRACT: Sealing is one of the most important process steps in industrial packaging, because the sealed seam is the most sensitive section of a package in terms of quality. For this reason, a major focus in flexible packaging is the sealing process, and among this, heat sealing is the most frequently used technology. In detail, applications of heat sealing processes are confronted with four conflicting objectives: increasing seam quality, reducing dwell time, reducing sealing temperature, and increasing process robustness towards varying conditions. Typical problems, such as identification of the optimum process parameters or selection of the most appropriate packaging film, are subject to these conflicting objectives.This paper presents a recently published design of experiments for characterizing and comparing heat sealing properties of packaging films based on a multi-objective optimization algorithm. The approach provides easy-to-read charts showing all optimum sealing parameters with regard to the four essential objectives of heat sealing: seam quality, dwell time, sealing temperature, and process robustness. Three case studies show exemplary applications of the new approach: 1) analyzing transport damages of beverage powder packages; 2) identifying and comparing optimum sealing parameter of a standard, mono-material, and fiber based packaging film regarding tightness and visual properties of the produced sachets; and 3) analyzing the effect of additional aluminum layers on sealing characteristics regarding hot-tack.The new design of experiments may provide the basis of a standard test method for the identification of optimal sealing parameters in the heat sealing processes.

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Open Access
Non-process elements in the recovery cycle of six Finnish kraft pulp mills, TAPPI Journal March 2023

ABSTRACT: In this work, the aim was to study the distribution and accumulation of the non-process elements (NPEs) in the recovery cycle of Finnish pulp mills and look at whether the geographical location (North vs. South) correlates with the current Finnish NPE levels. In addition, a comparison to older similar Finnish measurements was made with an attempt to analyze the reasons behind differences in the most typical non-process elements, aluminum (Al), silicon (Si), calcium (Ca), phosphorus (P), magnesium (Mg), manganese (Mn), chlorine (Cl), and potassium (K), taking into account the main elements in the white liquor, sodium (Na) and sulfur (S). The extensive laboratory results gained in this study are from seven sampling points at six pulp mills and present analytical data of metal concentrations. The data obtained presents an update to previous NPE studies. The levels found did not statistically differ between North and South Finland. The NPE levels, apart from phosphorus, found in Finnish pulp mills today have not changed considerably compared to the levels in earlier investigations in the 1990s. In the newest data, the phosphorus concentration was consistently higher in the as fired black liquor, electrostatic precipitator (ESP) ash, lime mud, and green liquor than in the previous results. In addition, the levels of Al, Si, Ca, P, and Mg in recovery boiler ESP ash were consistently higher compared to the older results. As the mills start to close their systems more, a stronger accumulation of NPEs can be expected, increasing the likelihood of more operational problems in the process. Further understanding of where the NPEs accumulate and how they can be most effectively removed will be valuable knowledge in the future.

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Open Access
Modeling and parameter optimization of the papermaking processes by using regression tree model and full factorial design, TAPPI Journal February 2021

ABSTRACT: One of the major challenges in the pulp and paper industry is taking advantage of the large amount of data generated through its processes in order to develop models for optimization purposes, mainly in the papermaking, where the current practice for solving optimization problems is the error-proofing method. First, the multiple linear regression technique is applied to find the variables that affect the output pressure controlling the gap of the paper sheet between the rod sizer and spooner sections, which is the main cause of paper breaks. As a measure to determine the predictive capacity of the adjusted model, the coefficient of determination (R2) and s values for the output pressure were considered, while the variance inflation factor was used to identify and eliminate the collinearity problem. Considering the same amount of data available by using machine learning, the regression tree was the best model based on the root mean square error (RSME) and R2. To find the optimal operating conditions using the regression tree model as source of output pressure measurement, a full factorial design was developed. Using an alpha level of 5%, findings show that linear regression and the regression tree model found only four independent variables as significant; thus, the regression tree model demonstrated a clear advantage over the linear regression model alone by improving operating conditions and demonstrating less variability in output pressure. Furthermore, in the present work, it was demonstrated that the adjusted models with good predictive capacity can be used to design noninvasive experiments and obtain.

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Open Access
Understanding wet tear strength at varying moisture content in handsheets, TAPPI Journal January 2021

ABSTRACT: A laboratory study was conducted looking at the effects of moisture content on wet tear strength in handsheets. Three different wetting techniques were used to generate the wet tear (Elmendorf-type) data at varying moisture levels, from TAPPI standard conditions (dry) to over 60% moisture content (saturated). Unbleached hardwood and softwood fiber from full-scale kraft pulp production were used. The softwood fiber was refined using a Valley beater to reduce freeness. Handsheets were made with a blend of hardwood and softwood and with refined softwood, without the addition of wet-end chemistry. The resulting grams-force tear data obtained from the test was indexed with basis weight and plotted versus both moisture content and dryness. As moisture content levels in the handsheets increased, the wet tear strength also increased, reaching a critical maximum point. This marked a transition point on the graph where, beyond a critical moisture content level, the tear strength began to decline linearly as moisture increased. This pattern was repeated in handsheets made from a blend of hardwood and softwood and from 100% refined softwood.

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Open Access
The effect of microfibrillated cellulose on the wet-web strength of paper, TAPPI Journal January 2021

ABSTRACT: The wet-web strength of paper immediately after the press section of a paper machine is a critical factor in determining machine runnability. However, it is difficult to determine at commercial scale, because the web has to be broken and production interrupted in order to obtain a sample for measurement. The use of microfibrillated cellulose (MFC) is believed to increase wet-web strength, as it has allowed filler level increases of 10% or more on many commercial paper machines. In this paper, we describe a laboratory method for estimating the effect of MFC on wet sheet strength after press-ing, as well as actual measurements of wet-web strength from a pilot paper machine trial. These experiments have demonstrated the positive effect of MFC. At solids contents in the range typically observed after pressing, sheets with MFC at fixed filler content are significantly stronger, but also wetter, than those without it. When the use of MFC is combined with a typical increase in filler content, the wet web remains slightly stronger, but also becomes drier than the reference condition. These results are compatible with the theory put forward by van de Ven that wet-web strength is mainly a result of friction between entangled fibers, and they also suggest that the presence of MFC increases this friction.

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Open Access
A guide to eliminating baggy webs, TAPPI Journal June 2021

ABSTRACT: Slack or baggy webs can cause misregistration, wrinkles, and breaks in printing and converting operations. Bagginess appears as non-uniform tautness in the cross direction (CD) of a paper web. The underlying cause is uneven CD tension profiles, for which there are few remedies once the paper is made. Precision measurements of CD tension profiles combined with trials on commercial paper machines have shown that uniform CD distribution of moisture, basis weight, and caliper profiles at the reel are key to avoiding bagginess. However, the most important but infrequently measured factor is the CD moisture profile entering the dryer section. Wetter areas entering the dryers are permanently elongated more than dry areas, leading to greater slackness in the finished paper. In storage, wound-in tension can amplify baggy streaks in paper near the surface of a roll and adjacent to the core. Unwrapped or poorly wrapped rolls exposed to low humidity environments may have baggy centers caused by moisture loss from the roll edges.All of the factors that impact bagginess have been incorporated in a mathematical model that was used to interpret the observations from commercial trials and can be used as a guide to solve future problems.

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Open Access
Paper bending stiffness and web tension measurement from a running web using a vacuum and computer imaging, TAPPI Journal May 2023

ABSTRACT: A novel method for measuring the bending stiffness of paper online during manufacturing is introduced. The method uses photometric stereo imaging to detect the shape of the deflection surface caused by a controllable pressure difference over the paper’s surfaces. The hardware for the measurement is based on a combination of two existing sensors, which has accelerated and facilitated the development of the implementation. The deflection and loads are tied together by the governing differential equation for the bending of an orthotropic elastic plate with selected simplifications. An approach to resolve material parameters and in-plane loads without knowledge of traditional boundary conditions is suggested. The presented method was tested in a paper mill during manufacturing. For bending stiffnesses measured online, correlation coefficients 0.88 and 0.92 were obtained compared to state-of-the-art laboratory measurements. However, the results gained from a moving web are noisy and the data requires correction of the slope and an off-set. Although several issues remain to be resolved before the method can be considered as an accurate measurement for industrial use, the theoretical background, the performance of online implementation, and the results are promising. Possible causes for the observed discrepancies and the future development of the method are discussed.

Journal articles
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Open Access
Investigation of the influencing factors in odor emission from wet-end white water, TAPPI Journal October 2020

ABSTRACT: Emission of malodorous gases, such as volatile organic compounds (VOCs), hydrogen sulfide (H2S), and ammonia (NH3) during pulping and papermaking has caused certain harm to the air environment and human health. This paper investigated the influencing factors of odor emission from wet-end white water during the production of bobbin paper in a papermaking mill using old corrugated containers (OCC) as raw material. The concentration of malodorous gases emitted from wet-end white water was determined with pump-suction gas detectors. The results indicated that low temperature could limit the release of malodorous gases from white water. Specifically, no total volatile organic compounds (TVOC), H2S, and NH3 was detected at a temperature of 15°C. The concentrations of malodorous gases were slightly increased when temperature increased to 25°C. When temperature was 55°C, the released concentrations of TVOC, H2S, and NH3 were 22.3 mg/m3, 5.91 mg/m3, and 2.78 mg/m3, respectively. Therefore, the content of malodorous gases significantly increased with the temperature increase. The stirring of white water accelerated the release of malodorous gases, and the release rate sped up as the stirring speed increased. However, the total amount of malodorous gases released were basically the same as the static state. Furthermore, the higher the concentration of white water, the greater the amount of malodorous gases released. The pH had little influence on the TVOC release, whereas it significantly affected the release of H2S and NH3. With the increase of pH value, the released amount of H2S and NH3 gradually decreased. When pH reached 9.0, the release amount of H2S and NH3 was almost zero, proving that an alkaline condition inhibits the release of H2S and NH3.

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Open Access
Using novel DNA methods to achieve higher process efficiency and performance, TAPPI Journal January 2023

ABSTRACT: Uncontrolled microbiological activity is a challenge for recycled fiber (RCF) mills as it can have negative effects on production and end-product quality. The microbes that exist in these systems have been largely unknown, and the strategies employed to control microbiology have been non-specific. Understanding the specific microbial groups present in RCF mills, their properties, and where they exist, as well as having the ability to accurately measure the true troublemakers, are key to targeted control of the bad actors. In this study, we present the results of a global survey of over 40 RCF paper machines. The same RCF-specific problem-causing bacterial groups were found on different continents, including large densities of newly identified bacteria in paper processes. Those can degrade cellulose and starch, produce acids and odorous substances, and have a significant impact on fiber strength and additive consumption. We also demonstrate how modern DNA tools can quantify the impact of biocidal countermeasures against the actual troublemakers, including bacteria found to degrade cellulose during RCF pulp storage, which may be linked to a negative impact on end-product strength. These novel DNA tools give producers updated biocide program key performance indicators (KPIs) and actionable information to more effectively design and adjust microbiological control to achieve higher process efficiency and performance.

Journal articles
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Open Access
Advanced real-time digital microscopy of foaming processes, TAPPI Journal January 2023

ABSTRACT: The properties of aqueous foams play a major role in foam forming and foam coating. Inline real-time foam measurements provide highly desired opportunities for optimization and control of foaming processes. This paper presents inline digital microscopy measurements of aqueous foams in foaming processes. It presents methods for providing detailed information on foam quality parameters, such as foam density and foam homogeneity in real time from the process. In addition, this study evaluates the performance of transillumination and front-light illumination in imaging of foams. The tests show very good results for the transillumination approach. Limitations of the image-based optical technique are discussed, and the precision of bubble size distribution measurement is assessed with a certificated reference substance. The measured foam densities are compared against the reference foam densities in the range 100•300 g/L, providing a linear correlation with R2 value of 0.99. In the case of heterogenous foams with a wide bubble size distribution, the bubble size-dependent dimensionless depth of field must be taken into account to obtain accurate estimates of foam density. Bubble-scale foam homogeneity is described by the standard deviation of bubble size distribution in foam.